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乙二醇
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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-乙酰基芴-9-酮
合成路线
（共 18 条）
42136-05-0
2-乙酰基芴-9-酮
→
反应条件
86-73-7
芴
+
781-73-7
2-乙酰芴
反应条件
bromine in acetic acid
参考文献
Pershin; Grigory Nikolaevich; Bogdanova; Nadezhda Sergeevna; Nikolaeva; Irina Sergeevna; Maichuk; Jury Fedorovich; Abramishvili; Roza Isaakovna; Avazov; Teshabai Nazarovich; Uretskaya; Galina Yakovlevna; Anikina; Svetlana Jurievna; Grinev; Alexei Nikolaevich; Kraft; Maxim Yakovlevich
Patent: US4016289 A1, 1977 ;
42136-05-0
2-乙酰基芴-9-酮
→
反应条件
784-50-9
9-芴酮-2-羧酸
反应条件
暂无反应条件数据
参考文献
Koden; Takenaka; Kusabayashi
Molecular crystals and liquid crystals, 1982 , vol. 88, # 1-4 p. 137 - 150
42136-05-0
2-乙酰基芴-9-酮
→
反应条件
86-73-7
芴
+
781-73-7
2-乙酰芴
反应条件
bromine in acetic acid
参考文献
Pershin; Grigory Nikolaevich; Bogdanova; Nadezhda Sergeevna; Nikolaeva; Irina Sergeevna; Maichuk; Jury Fedorovich; Abramishvili; Roza Isaakovna; Avazov; Teshabai Nazarovich; Uretskaya; Galina Yakovlevna; Anikina; Svetlana Jurievna; Grinev; Alexei Nikolaevich; Kraft; Maxim Yakovlevich
Patent: US4016289 A1, 1977 ;
781-73-7
2-乙酰芴
→
反应条件
42136-05-0
2-乙酰基芴-9-酮
反应条件
N-benzyl-trimethylammonium hydroxide in pyridine; methanol T=20°C; 3 h;
参考文献
Minabe, Masahiro; Yamazaki, Ayumi; Imai, Toshinobu; Takanezawa, Takumi; Karikomi, Michinori
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 11 p. 1758 - 1765
107942-87-0
→
反应条件
42136-05-0
2-乙酰基芴-9-酮
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; trimethylacetic anhydride; 1,2-bis-(diphenylphosphino)ethane; potassium iodide T=160°C; 0.5 h; Inert atmosphereMicrowave irradiationSealed tube; Wavelength;
参考文献
Fukuyama, Takahide; Maetani, Shinji; Miyagawa, Kazusa; Ryu, Ilhyong
Organic Letters, 2014 , vol. 16, # 12 p. 3216 - 3219
→
反应条件
42136-05-0
2-乙酰基芴-9-酮
反应条件
sulfuric acid in water; acetic acid
参考文献
Pershin; Grigory Nikolaevich; Bogdanova; Nadezhda Sergeevna; Nikolaeva; Irina Sergeevna; Maichuk; Jury Fedorovich; Abramishvili; Roza Isaakovna; Avazov; Teshabai Nazarovich; Uretskaya; Galina Yakovlevna; Anikina; Svetlana Jurievna; Grinev; Alexei Nikolaevich; Kraft; Maxim Yakovlevich
Patent: US4016289 A1, 1977 ;
113770-25-5
→
反应条件
42136-05-0
2-乙酰基芴-9-酮
+
274249-30-8
反应条件
potassium hydroxide in methanol; acetone T=20°C; Dimerization; 1 h;
参考文献
Minabe, Masahiro; Oba, Toru; Tanaka, Masayuki; Kanno, Keiko; Tsubota, Motohiro
Chemistry Letters, 2000 , # 5 p. 498 - 499
610-97-9
2-碘苯甲酸甲酯
→
反应条件
42136-05-0
2-乙酰基芴-9-酮
反应条件
1: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran; water / 12 h / 60 °C / |Inert atmosphere 2: sodium hydroxide / water; methanol / 12 h / 20 °C 3: 1,2-bis-(diphenylphosphino)ethane; trimethylacetic anhydride; [RhCl(η2:η2-cycloocta-1,5-diene)]2; potassium iodide / 0.5 h / 160 °C / |Inert atmosphere; |Microwave irradiation; |Sealed tube View Scheme
参考文献
Fukuyama, Takahide; Maetani, Shinji; Miyagawa, Kazusa; Ryu, Ilhyong
Organic Letters, 2014 , vol. 16, # 12 p. 3216 - 3219
148651-41-6
→
反应条件
42136-05-0
2-乙酰基芴-9-酮
反应条件
1: sodium hydroxide / water; methanol / 12 h / 20 °C 2: 1,2-bis-(diphenylphosphino)ethane; trimethylacetic anhydride; [RhCl(η2:η2-cycloocta-1,5-diene)]2; potassium iodide / 0.5 h / 160 °C / |Inert atmosphere; |Microwave irradiation; |Sealed tube View Scheme
参考文献
Fukuyama, Takahide; Maetani, Shinji; Miyagawa, Kazusa; Ryu, Ilhyong
Organic Letters, 2014 , vol. 16, # 12 p. 3216 - 3219
149104-90-5
4-乙酰基苯硼酸
→
反应条件
42136-05-0
2-乙酰基芴-9-酮
反应条件
1: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran; water / 12 h / 60 °C / |Inert atmosphere 2: sodium hydroxide / water; methanol / 12 h / 20 °C 3: 1,2-bis-(diphenylphosphino)ethane; trimethylacetic anhydride; [RhCl(η2:η2-cycloocta-1,5-diene)]2; potassium iodide / 0.5 h / 160 °C / |Inert atmosphere; |Microwave irradiation; |Sealed tube View Scheme
参考文献
Fukuyama, Takahide; Maetani, Shinji; Miyagawa, Kazusa; Ryu, Ilhyong
Organic Letters, 2014 , vol. 16, # 12 p. 3216 - 3219
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