2,4-二甲基-1-碘苯合成路线 （共 38 条）
反应条件
formaldehyd; palladium diacetate; caesium carbonate in dimethyl sulfoxide T=80°C; 12 h;
参考文献
Pyo, Ayoung; Kim, Sudeok; Kumar, Manian Rajesh; Byeun, Aleum; Eom, Min Sik; Han, Min Su; Lee, Sunwoo
Tetrahedron Letters, 2013 , vol. 54, # 38 p. 5207 - 5210
参考文献
Klages; Liecke
Journal fuer Praktische Chemie (Leipzig), 1900 , vol. <2> 61, p. 322
参考文献
Edinger; Goldberg
Chemische Berichte, 1900 , vol. 33, p. 2884
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Grahl
Chemische Berichte, 1895 , vol. 28, p. 89
反应条件
1: 96 percent / H2; CuI; triethylamine / dichlorobis(triphenylphosphine)palladium(II) / 2 h / 20 °C 2: 92 percent / KOH / methanol / 3 h View Scheme
参考文献
Elangovan, Arumugasamy; Wang, Yu-Hsiang; Ho, Tong-Ing
Organic Letters, 2003 , vol. 5, # 11 p. 1841 - 1844
反应条件
[NiCl(1-naph)(PPh3)2]; sodium hydride; triphenylphosphine in toluene; white oil T=120°C; 12 h; Inert atmosphere;
参考文献
Gao, Cai-Yan; Cao, Xingbo; Yang, Lian-Ming
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 19 p. 3922 - 3925
反应条件
palladium diacetate; potassium carbonate in methoxybenzene T=140°C; Suzuki coupling; 12 h;
参考文献
Jafarpour, Farnaz; Rashidi-Ranjbar, Parviz.; Kashani, Asieh Otaredi
European Journal of Organic Chemistry, 2011 , # 11 p. 2128 - 2132
反应条件
1: With copper(l) iodide; 2-methyl-8-hydroxyquinoline; tetra(n-butyl)ammonium hydroxide in water; dimethyl sulfoxide T=100°C; 10 h; 2: With hydrogenchloride in water; N,N-dimethyl-formamide T=20°C;
参考文献
Paul, Rajesh; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Synthesis, 2010 , # 24 art. no. P11610SS, p. 4268 - 4272
反应条件
potassium hydroxide; tetrabutylammomium bromide; copper(l) iodide in water T=80°C; 12 h;
参考文献
Rout, Laxmidhar; Saha, Prasenjit; Jammi, Suribabu; Punniyamurthy, Tharmalingam
European Journal of Organic Chemistry, 2008 , # 4 p. 640 - 643
反应条件
potassium hydroxide in dimethyl sulfoxide T=80°C; 40 h; air;
参考文献
Jammi, Suribabu; Sakthivel, Sekarpandi; Rout, Laxmidhar; Mukherjee, Tathagata; Mandai, Santu; Mitra, Raja; Saha, Prasenjit; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2009 , vol. 74, # 5 p. 1971 - 1976
参考文献
Couture, Christiane; Paine, Anthony James
Canadian Journal of Chemistry, 1985 , vol. 63, p. 111 - 120
