1-环丙基-1-(三甲基硅烷基氧基)-乙烯合成路线 （共 10 条）
反应条件
sodium hydroxide; water; acetic acid; sodium chloride in acetonitrile T=25°C; Rate constantMechanism;
参考文献
Novice, Marilyn H.; Seikaly, Hani R.; Seiz, Annette D.; Tidwell, Thomas T.
Journal of the American Chemical Society, 1980 , vol. 102, # 18 p. 5835 - 5838
反应条件
sodium hydroxide; water; acetic acid; sodium chloride in acetonitrile T=25°C; Rate constantMechanism;
参考文献
Novice, Marilyn H.; Seikaly, Hani R.; Seiz, Annette D.; Tidwell, Thomas T.
Journal of the American Chemical Society, 1980 , vol. 102, # 18 p. 5835 - 5838
反应条件
zinc(II) chloride in dichloromethane other aldehydes;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 1.2 p. 208
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 225 - 226
反应条件
T=110°C; ΔH(activation), ΔS(activation), ΔG(activation) for 350 deg C; Thermodynamic dataKineticsRate constant;
参考文献
Journal of Organic Chemistry, , vol. 46, # 3 p. 506 - 509
反应条件
in benzene
T=10 - 15°C; 4 h; Irradiation; Yields of byproduct given;
参考文献
Shimizu, Nobujiro; Yamaoka, Shintaro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3853 - 3854
反应条件
in acetonitrile
T=-25°C; 24 h; Irradiation;
参考文献
Gan, Chee Yong; Lambert, John N.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 15 p. 2363 - 2372
反应条件
in benzene
T=10 - 15°C; 4 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Shimizu, Nobujiro; Yamaoka, Shintaro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3853 - 3854
反应条件
1: 80 percent / benzene / 4 h / 10 - 15 °C / Irradiation
2: 90 percent / K2CO3 / methanol / 24 h / Ambient temperature
View Scheme
参考文献
Shimizu, Nobujiro; Yamaoka, Shintaro; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 12 p. 3853 - 3854
反应条件
1: 71 percent / ZnCl2 / CH2Cl2 / 2 h / 20 °C
2: 88 percent / TsOH*H2O / benzene / 0.33 h / Heating
3: H2 / Raney-Ni / ethanol / 4 h / 25 °C / 760 Torr
View Scheme
参考文献
Cheskis, B. A.; Ivanova, N. M.; Moiseenkov, A. M.; Nefedov, O. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 9.1. p. 1839 - 1849
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 9 p. 2025 - 2036
反应条件
(difluoroiodo)benzene-boron trifluoride in dichloromethane
T=-78 - 20°C;
参考文献
Zefirov, N. S.; Samoniya, N. Sh.; Kutateladze, T. G.; Zhdankin, V. V.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 1.2 p. 194 - 195
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 1 p. 220 - 222
