N1,N2-二(苯基甲基)-1,2-丙烷二胺合成路线 （共 5 条）
反应条件
1: in methanol
T=0 - 20°C; 2.5 h;
2: With methanol; sodium tetrahydroborate
T=0 - 20°C; 16 h;
参考文献
LEO PHARMA A/S; NIELSEN, Simon, Feldbaek; GREVE, Daniel, Rodriguez; GRUE-SOERENSEN, Gunnar; RYTTERSGAARD, Carsten; SCHOU, Soeren, Christian; SAMS, Anette, Graven
Patent: WO2012/3829 A1, 2012 ;
Location in patent: Page/Page column 66-67 ;
WO 2012/003829 A1
反应条件
sodium hydrogencarbonate; [{(η5-C5Me5)IrCl}2(μ-Cl)2] in water
T=140°C; 15 h;
参考文献
Nordstrom, Lars Ulrik; Madsen, Robert
Chemical Communications, 2007 , # 47 p. 5034 - 5036
反应条件
sodium tetrahydroborate in methanol
T=20°C; 1 h;
参考文献
Andrianina Ralambomanana, Dimby; Razafimahefa-Ramilison, Dorothee; Rakotohova, Andry Clement; Maugein, Jeanne; Pelinski, Lydie
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 21 p. 9546 - 9553
反应条件
[{(η5-C5Me5)IrCl}2(μ-Cl)2]; sodium hydrogencarbonate in water
T=140°C; 15 h; Inert atmosphere;
参考文献
Lorentz-Petersen, Linda L. R.; Nordstrom, Lars Ulrik; Madsen, Robert
European Journal of Organic Chemistry, 2012 , # 34 p. 6752 - 6759
参考文献
Dow Chem.Co.
Patent: US2753355 , 1955 ;
