(R)-(+)-萘基-1-乙醇合成路线 (共 74 条)
反应条件
Candida parapsilosis MTCC 1965 in aq. phosphate buffer T=30°C; pH=7; 12 h; Microbiological reaction; TemperatureTimepH-valueSolvent; stereoselective reaction;
参考文献
Amrutkar, Suyog Madhav; Banoth, Linga; Banerjee, Uttam Chand
Tetrahedron Letters, 2013 , vol. 54, # 25 p. 3274 - 3277
反应条件
(1R)-N-oxyl-1-(N-benzylcarbamoyl)-8-azabicyclo[3.2.1]octane; sodium hydrogencarbonate; sodium bromide in dichloromethane; water T=0°C; Electrochemical reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Demizu, Yosuke; Shiigi, Hirofumi; Mori, Hiroyuki; Matsumoto, Kazuya; Onomura, Osamu
Tetrahedron Asymmetry, 2008 , vol. 19, # 23 p. 2659 - 2665
反应条件
potassium hydroxide; hydrogen; DM-DABN; [RuCl2((R)-3,3'-dm-binap)(dmf)n]; (1S,2S)-(-)-1,2-diphenylethylenediamine in isopropyl alcohol T=20°C; P=6080 Torr; 4 h;
参考文献
Mikami, Koichi; Korenaga, Toshinobu; Ohkuma, Takeshi; Noyori, Ryoji
Angewandte Chemie - International Edition, 2000 , vol. 39, # 20 p. 3707 - 3710
反应条件
dimethylsulfide borane complex; (S)-2-(anilinodiphenylmethyl)pyrrolidine in tetrahydrofuran T=20°C; 2 h; enantioselective reaction;
参考文献
Hosoda, Naoya; Kamito, Hideaki; Takano, Miki; Takebe, Yoshitaka; Yamaguchi, Yoshitaka; Asami, Masatoshi
Tetrahedron, 2013 , vol. 69, # 11 p. 2509 - 2509
反应条件
Candida antarctica lipase B; (η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate; sodium carbonate in tetrahydrofuran; toluene T=20°C; 24 h;
参考文献
Martin-Matute, Belen; Edin, Michaela; Bogar, Krisztian; Kaynak, F. Betuel; Baeckvall, Jan-E.
Journal of the American Chemical Society, 2005 , vol. 127, # 24 p. 8817 - 8825
反应条件
tricarbonyl(η6-arene)chromium(0) complex derived from (1S,2R)-N,N-dibutylnorephedrine in hexane; toluene T=0°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sprout, Christopher M.; Seto, Christopher T.
Journal of Organic Chemistry, 2003 , vol. 68, # 20 p. 7788 - 7794
反应条件
phosphate buffer in diethyl ether 65 h; Ambient temperaturebovine liver acetone powder (BLAP); Yield given. Yields of byproduct given;
参考文献
Houiene, Zahia; Merabet-Khelassi, Mounia; Bouzemi, Nassima; Riant, Olivier; Aribi-Zouioueche, Louisa
Tetrahedron Asymmetry, 2013 , vol. 24, # 5-6 p. 290 - 296
反应条件
Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mczka, Wanda K; Mironowicz, Agnieszka
Tetrahedron Asymmetry, 2002 , vol. 13, # 21 p. 2299 - 2302
反应条件
titanium(IV) isopropylate; (R,S)-2-OH-3,5-Cl2-C6H2-SO2-NH-CH(CH2Ph)-CH(Ph)OH in tetrahydrofuran T=0°C; 12 h;
参考文献
You; Hsieh; Gau
Chemical Communications, 2001 , # 17 p. 1546 - 1547
反应条件
triethylamine; (-)-diethyl[3-(2-phenylnaphthyl)(4-pyridyl)]amine in toluene T=-78°C; 9 h; Title compound not separated from byproducts;
参考文献
Birman, Vladimir B.; Li, Ximin
Organic Letters, 2006 , vol. 8, # 7 p. 1351 - 1354