2,2,3,3,3-五氟-1-丙醇合成路线 （共 52 条）
参考文献
McBee et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 86
反应条件
(i) NaH, Et2O, (ii) (NPCl2)3, toluene; Multistep reaction;
参考文献
Allcock,H.R.; Walsh,E.J.
Journal of the American Chemical Society, 1972 , vol. 94, p. 119 - 124
反应条件
pyridine in chloroform T=0 - 20°C;
参考文献
WO2004/9528 A1, ;
Page 27 ;
反应条件
potassium hydroxide in water T=75 - 85°C; P=5250.53 - 6000.6 Torr; Inert atmosphereAutoclave;
参考文献
Daikin Industries, Ltd.
Patent: EP2305626 A1, 2011 ;
Location in patent: Page/Page column 13-14 ;
反应条件
Nafion; phosphoric acid T=95°C; 10 h; Pervaporation composite membrane made from polyvinylalcohol and glutaraldehyde; Conversion of starting material;
参考文献
KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY
Patent: US2005/85661 A1, 2005 ;
Location in patent: Page/Page column 4 ;
反应条件
1: With titanium tetrachloride T=35°C; 0.666667 h; Inert atmosphere; 2: With zinc in diethylene glycol dimethyl ether T=85°C; 3 h; Cooling with ice;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY; STEPANOV, Andrei, Aleksandrovich; CHERSTKOV, Victor, Filippovich; NAPPA, Mario, Joseph
Patent: WO2011/90734 A1, 2011 ;
Location in patent: Page/Page column 7 ;
反应条件
methane; nickel T=497 - 579°C; P=822.11 Torr; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US7026520 B1, 2006 ;
Location in patent: Page/Page column 3-4 ;
反应条件
hydrogen; 3 Pd/C T=414°C; Inert atmosphereGas phase; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.; KOMATSU, Yuzo; SUGIYAMA, Akinari; SHIBANUMA, Takashi
Patent: WO2010/87465 A1, 2010 ;
Location in patent: Page/Page column 13 ;
反应条件
hydrogen; carbon Inert atmosphereGas phase; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.; KOMATSU, Yuzo; SUGIYAMA, Akinari; SHIBANUMA, Takashi
Patent: WO2010/87465 A1, 2010 ;
Location in patent: Page/Page column 12-13 ;
反应条件
methane; nickel T=497 - 579°C; P=822.11 Torr; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US7026520 B1, 2006 ;
Location in patent: Page/Page column 3-4 ;
