1,2-二氯-1,1,2,3,3-五氟-丙烷合成路线 (共 8 条)
参考文献
Fainberg; Miller
Journal of the American Chemical Society, 1957 , vol. 79, p. 4170,4174
反应条件
acetic anhydride; zinc in dichloromethane
T=40°C; 10 h;
参考文献
Wlassics, Ivan; Tortelli, Vito
Collection of Czechoslovak Chemical Communications, 2008 , vol. 73, # 12 p. 1719 - 1728
反应条件
acetic anhydride; zinc in dichloromethane
T=40°C;
参考文献
Wlassics, Ivan; Tortelli, Vito
Collection of Czechoslovak Chemical Communications, 2008 , vol. 73, # 12 p. 1719 - 1728
参考文献
Fainberg; Miller
Journal of the American Chemical Society, 1957 , vol. 79, p. 4170,4174
反应条件
aluminium trichloride
T=0 - 10°C; 10 h; Further byproducts given;
参考文献
Tanuma, T.; Ohnishi, K.; Okamoto, H.; Miyajima, T.; Morikawa, S.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 259 - 284
反应条件
triethylsilane; meta-chloroperoxybenzoic acid
1) 25 deg C, 1 h, 2) 100 deg C, 12 h; Yield givenFurther byproducts given. Yields of byproduct given;
参考文献
Petrov, Viacheslav A.
Journal of Organic Chemistry, 1998 , vol. 63, # 21 p. 7294 - 7297
反应条件
triethylsilane; meta-chloroperoxybenzoic acid
1) 25 deg C, 1 h, 2) 100 deg C, 12 h; Yield givenFurther byproducts given. Yields of byproduct given;
参考文献
Petrov, Viacheslav A.
Journal of Organic Chemistry, 1998 , vol. 63, # 21 p. 7294 - 7297
参考文献
Hauptschein; Bigelow
Journal of the American Chemical Society, 1951 , vol. 73, p. 1428