3-[(三甲基硅烷基)氧基]丙腈合成路线 (共 5 条)
反应条件
pyridine; phosphorus trichoride in dichloromethane T=-65 - 20°C; 336 h; Inert atmosphereSealed tube;
参考文献
Majewski, Piotr
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 4 p. 942 - 955
反应条件
phosphorus trichoride in acetonitrile 48 h; Ambient temperature;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 7, # 24 p. 3171 - 3176
反应条件
Ammonium thiocyanate in dichloromethane
T=0°C; 0.166667 h;
参考文献
Jadhav, Vrushali H.; Kumar, K. S. Ajish; Chaudhari, Vinod D.; Dhavale, Dilip D.
Synthetic Communications, 2007 , vol. 37, # 8 p. 1363 - 1370
参考文献
Krolevets, A. A.; Antipova, V. V.; Popov, A. G.; Adamov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 10 p. 2274 - 2281,2023 - 2030
反应条件
DIBAO-i-Pr in hexane
Ambient temperatureother oxiranes; var. Lewis acids; var. solvents; var. temperatures; Product distribution;
参考文献
Imi, Katsuharu; Yanagihara, Naoto; Utimoto, Kiitiro
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 1013 - 1016