Alpha-氯-4-氟苯甲醛肟合成路线 （共 15 条）
反应条件
1: With triethylamine in trichloroethane, 1,1,2-
0.5 h; Heating;
2: With sodium hydroxide
0.5 h; Heating;
参考文献
Schofield, Mark H.; Sorel, Marie-Adele; Manalansan, Ryan J.; Richardson, David P.; Markgraf, J. Hodge
Magnetic Resonance in Chemistry, 2006 , vol. 44, # 9 p. 851 - 855
反应条件
triethylamine in dichloromethane
T=20°C; 6 h;
参考文献
Xu, Wei Ming; Tang; Huang, Xian
Tetrahedron, 2005 , vol. 61, # 2 p. 501 - 506
反应条件
triethylamine in dichloromethane
T=20°C; 6 h;
参考文献
Xu, Wei Ming; Tang; Huang, Xian
Tetrahedron, 2005 , vol. 61, # 2 p. 501 - 506
反应条件
1: 38 percent / Et3N / diethyl ether / 0.75 h
2: conc. aq. HCl, CH3COOH / 72 h / Heating
3: oxalyl chloride, DMF / CH2Cl2 / 1 h / Heating
View Scheme
参考文献
Hamper, Bruce C.; Leschinsky, Kindrick L.; Massey, Steven S.; Bell, Crystal L.; Brannigan, Lawrence H.; Prosch, S. Douglas
Journal of Agricultural and Food Chemistry, 1995 , vol. 43, # 1 p. 219 - 228
反应条件
1: 73 percent / triethylamine / CH2Cl2 / 6 h / 20 °C
2: CH3I; NaI / dimethylformamide / 20 h / 80 °C
3: DBU / tetrahydrofuran; dimethylformamide / 10 h / 90 °C
View Scheme
参考文献
Xu, Wei Ming; Tang; Huang, Xian
Tetrahedron, 2005 , vol. 61, # 2 p. 501 - 506
