1-(4-甲基苯基)-3-苯基丙-2-烯-1-酮合成路线 (共 63 条)
反应条件
1: 86 percent / EtONa / ethanol / 1 h / Heating 2: Se / 0.5 h / 180 - 200 °C View Scheme
参考文献
Sabri, Salim S.; Hussein, Ahmad Q.; Al-Hajjar, Farouk H.
Journal of Chemical & Engineering Data, 1985 , vol. 30, # 4 p. 512 - 514
反应条件
1: 68 percent / CH2Cl2 / 40 - 42 °C 2: 62 percent / KOH / ethanol / Heating View Scheme
参考文献
Synlett, , # 14 p. 2189 - 2192
参考文献
Helvetica Chimica Acta, , vol. 57, # 7 p. 2201 - 2209
反应条件
samarium in N,N-dimethyl-formamide T=25°C; Michael addition; 1.5 h; Inert atmosphere;
参考文献
Liu, Yongjun; Li, Yuanying; Qi, Yan; Wan, Jun
Synthesis, 2010 , # 24 art. no. F12610SS, p. 4188 - 4192
反应条件
1: With C20H24F6MnN4O6S2 in acetonitrile T=20°C; 0.05 h; Inert atmosphere; 2: With peracetic acid in acetonitrile T=20°C; 1.33333 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Bin; Miao, Cheng-Xia; Wang, Shou-Feng; Kuehn, Fritz E.; Xia, Chun-Gu; Sun, Wei
Journal of Organometallic Chemistry, 2012 , vol. 715, p. 9 - 12
反应条件
1: With C28H34F6MnN6O6S2; acetic acid in acetonitrile 0.0833333 h; Inert atmosphere; 2: With dihydrogen peroxide in acetonitrile T=-20 - 20°C; 2 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Bin; Miao, Chengxia; Wang, Shoufeng; Xia, Chungu; Sun, Wei
Chemistry - A European Journal, 2012 , vol. 18, # 22 p. 6750 - 6753
反应条件
1: With C20H24F6MnN4O6S2 in acetonitrile T=20°C; 0.05 h; Inert atmosphere; 2: With peracetic acid in acetonitrile T=20°C; 1.33333 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Bin; Miao, Cheng-Xia; Wang, Shou-Feng; Kuehn, Fritz E.; Xia, Chun-Gu; Sun, Wei
Journal of Organometallic Chemistry, 2012 , vol. 715, p. 9 - 12
反应条件
1: With C28H34F6MnN6O6S2; acetic acid in acetonitrile 0.0833333 h; Inert atmosphere; 2: With dihydrogen peroxide in acetonitrile T=-20 - 20°C; 2 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Bin; Miao, Chengxia; Wang, Shoufeng; Xia, Chungu; Sun, Wei
Chemistry - A European Journal, 2012 , vol. 18, # 22 p. 6750 - 6753
反应条件
potassium superoxide in acetonitrile 0.25 h; Irradiation;
参考文献
Chemistry Letters, , p. 519 - 520
反应条件
potassium superoxide 0.25 h; Irradiation;
参考文献
Chemistry Letters, , p. 519 - 520