1-(4-甲基苯基)-3-苯基丙-2-烯-1-酮合成路线 (共 63 条)
反应条件
thionyl chloride in ethanol
T=20°C;
参考文献
Hu, Zhiguo; Liu, Jun; Dong, Zhibing; Guo, Lili; Wang, Dong; Zeng, Pingli
Journal of Chemical Research, 2004 , # 2 p. 158 - 159
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; 2-(di-1-adamantylphosphanyl)-1-(2,6-diisopropylphenyl)-1H-imidazole; triethylamine in 1,4-dioxane
T=100°C; P=3750.38 Torr; 20 h; Inert atmosphereAutoclave;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
European Journal of Organic Chemistry, 2011 , # 25 p. 4919 - 4924
反应条件
IPrAuNTf2 in methanol; water
T=50°C; Meyer-Schuster Rearrangement; 2 h;
参考文献
Hansmann, Max M.; Hashmi, A. Stephen K.; Lautens, Mark
Organic Letters, 2013 , vol. 15, # 13 p. 3226 - 3229
反应条件
sodium ethanolate in ethanol
4 h; Heating;
参考文献
Dora; Dash; Panda
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 3 p. 691 - 696
反应条件
TeCl4 in dichloromethane
2 h; Ambient temperature;
参考文献
Tani, Hiroyuki; Inamasu, Tokuo; Masumoto, Kazunori; Tamura, Rui; Shimizu, Hiroshi; Suzuki, Hitomi
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 67, # 1-4 p. 261 - 266
反应条件
ammonium acetate in ethanol
1.25 h; Heating;
参考文献
Selvaraj, Sangavanaicker; Dhanabalan, Anantharaman; Arumugam, Natesan
Tetrahedron Letters, 1991 , vol. 32, # 50 p. 7469 - 7470
反应条件
1: acetylacetone With ethanol; sodium ethanolate
2: C32H26O2S in ethanol; N,N-dimethyl-formamide
T=20°C; 1 h; stereoselective reaction;
参考文献
Vinosha, Beer Mohamed; Renuga, Subbiah; Gnanadeebam, Michael; Perumal, Subbu; Lycka, Antonin
Synthetic Communications, 2009 , vol. 39, # 15 p. 2776 - 2788
反应条件
selenium(IV) oxide in ethanol
24 h; Reflux; regioselective reaction;
参考文献
Khurana, Jitender M.; Dawra, Kiran; Majumdar, Susruta
Monatshefte fur Chemie, 2009 , vol. 140, # 1 p. 69 - 72
反应条件
1,3-bis-(diphenylphosphino)propane; palladium diacetate in dimethyl sulfoxide
T=60°C; 20 h; Autoclave;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Chemistry - An Asian Journal, 2012 , vol. 7, # 2 p. 282 - 285
反应条件
C-200 (barium hydroxide) in 1,4-dioxane; water
T=76°C; 1 h;
参考文献
Sinisterra, J. V.; Marinas, J. M.; Riquelme, F.; Arias, M. S.
Tetrahedron, 1988 , vol. 44, # 5 p. 1431 - 1440