1-(4-甲基苯基)-3-苯基丙-2-烯-1-酮合成路线 （共 63 条）
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C
1.2: 5 h / 0 - 20 °C
2.1: IPrAuNTf2 / methanol; water / 2 h / 50 °C
View Scheme
参考文献
Hansmann, Max M.; Hashmi, A. Stephen K.; Lautens, Mark
Organic Letters, 2013 , vol. 15, # 13 p. 3226 - 3229
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C
1.2: 5 h / 0 - 20 °C
2.1: IPrAuNTf2 / methanol; water / 2 h / 50 °C
View Scheme
参考文献
Hansmann, Max M.; Hashmi, A. Stephen K.; Lautens, Mark
Organic Letters, 2013 , vol. 15, # 13 p. 3226 - 3229
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; water
T=20°C;
参考文献
Khurana, Jitender M.; Dawra, Kiran; Majumdar, Susruta
Monatshefte fur Chemie, 2009 , vol. 140, # 1 p. 69 - 72
反应条件
samarium (III) iodide in tetrahydrofuran
T=20°C;
参考文献
Fan, Xuesen; Zhang, Yongmin
Journal of Chemical Research - Part S, 2001 , # 3 p. 104 - 105
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide
0.5 h; Heating;
参考文献
Khurana; Bansal; Chauhan
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 6 p. 1089 - 1091
反应条件
1: methanol; sodium tetrahydroborate / 2 h / 0 - 10 °C / Inert atmosphere
2: [Ir2(COD)2(SnCl3)2(Cl)2(μ-Cl)2] / 1,2-dichloro-ethane / 0.75 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2012 , vol. 68, # 19 p. 3776 - 3785
反应条件
1: sodium hydroxide / ethanol; water / 4 h / 0 - 20 °C / Inert atmosphere
2: methanol; sodium tetrahydroborate / 2 h / 0 - 10 °C / Inert atmosphere
3: [Ir2(COD)2(SnCl3)2(Cl)2(μ-Cl)2] / 1,2-dichloro-ethane / 0.75 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2012 , vol. 68, # 19 p. 3776 - 3785
反应条件
1: sodium hydroxide / ethanol; water / 4 h / 0 - 20 °C / Inert atmosphere
2: methanol; sodium tetrahydroborate / 2 h / 0 - 10 °C / Inert atmosphere
3: [Ir2(COD)2(SnCl3)2(Cl)2(μ-Cl)2] / 1,2-dichloro-ethane / 0.75 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2012 , vol. 68, # 19 p. 3776 - 3785
参考文献
Ch. Mayer
Bulletin de la Societe Chimique de France, 1905 , vol. <3> 33, p. 397
反应条件
1: Br2
2: NaOMe / methanol
View Scheme
参考文献
Dayer,F. et al.
Helvetica Chimica Acta, 1974 , vol. 57, # 7 p. 2201 - 2209
