1,2-(二十二烷氧荃)苯合成路线 (共 12 条)
反应条件
N-bromosuccinmide in tetrahydrofuran T=0°C; Darkness; regioselective reaction;
参考文献
Zhao, Baomin; Liu, Bo; Png, Rui Qi; Zhang, Kai; Lim, Kheng Aik; Luo, Jing; Shao, Jinjun; Ho, Peter K.H.; Chi, Chunyan; Wu, Jishan
Chemistry of Materials, 2010 , vol. 22, # 2 p. 435 - 449
反应条件
1: 72 percent / nitric acid; acetic acid / CH2Cl2; H2O / 0 - 20 °C 2: 90 percent / hydrogen / Pd/C / ethanol / 24 h / 1520 Torr / Heating View Scheme
参考文献
Wicklein, Andre; Muth, Mathis-Andreas; Thelakkat, Mukundan
Journal of Materials Chemistry, 2010 , vol. 20, # 39 p. 8646 - 8652
反应条件
carbon disulfide; AlCl3, aluminium chloride T=0°C; 8 h; Inert atmosphere;
参考文献
Chen, Chun-Jung; Wu, Yu-Che; Sheu, Hwo-Shuenn; Lee, Gene-Hsiang; Lai, Chung K.
Tetrahedron, 2011 , vol. 67, # 1 p. 114 - 124
反应条件
bromine in dichloromethane T=25°C; 2 h;
参考文献
Pol, J. F. van der; Neeleman, E.; Zwikker, J. W.; Nolte, R. J. M.; Drenth, W.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, p. 615 - 620
反应条件
potassium carbonate in acetone
Williamson ether synthesis; 48 h; Reflux;
参考文献
Hope-Ross, Kyle A.; Heiney, Paul A.; Kadla, John F.
Canadian Journal of Chemistry, 2010 , vol. 88, # 7 p. 639 - 645
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=60°C; 48 h;
参考文献
Clarkson, Guy J.; McKeown, Neil B.; Treacher, Kevin E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 14 p. 1817 - 1824
反应条件
potassium carbonate; potassium iodide
Williamson etherification reaction; 10 h; Heating;
参考文献
Diaz Diaz, David; Torres, Tomas; Zentel, Rudolf; Davis, Riju; Brehmer, Martin
Chemical Communications, 2007 , # 23 p. 2369 - 2371
反应条件
1: C5H5N / 0 - 5 °C
2: t-BuOK / propan-2-ol
View Scheme
参考文献
Guemues, G.; Ahsen, V.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 348, p. 167 - 178
反应条件
potassium tert-butylate in isopropyl alcohol
参考文献
Guemues, G.; Ahsen, V.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 348, p. 167 - 178
反应条件
potassium hydroxide; Aliquatreg; 336
参考文献
Strzelecka, H.; Jallabert, C.; Veber, M.; Davidson, P.; Levelut, A. M.
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 161, p. 395 - 402