反应条件
in tetrahydrofuran; diethyl ether addn. of tributyltin lithium soln. (prepared in situ from Li and (n-Bu)3SnCl in THF) at -7°C to soln. of the propane in dry ether, mixt.immediately turned white, stirred (2h), refluxed (1h); addn. of water, extd. with CH2Cl2, organic layer dried (MgSO4), evapn. (vac.), bulb to bulb distn. (120°C, 0.1 mmHg) of yellow liq., flash chromy. (Florisil, pentane), addn. of ethylacetate/hexane (2/5);
参考文献
Suggs, J. William; Lee, Ken. S.
Journal of Organometallic Chemistry, 1986 , vol. 299, p. 297 - 310
