N-(4-(2,5-二氧代-4-恶唑烷基)丁基)-2,2,2-三氟乙酰胺合成路线 （共 8 条）
反应条件
in tetrahydrofuran T=25°C; 4 h;
参考文献
Blacklock; Shuman; Butcher; Shearin Jr.; Budavari; Grenda
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 836 - 844
反应条件
in 1,4-dioxane T=45°C; 2 h;
参考文献
Cherevin; Gulevich; Popova; Zubreichuk; Knizhnikov
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 10 p. 1427 - 1431
反应条件
in ethyl acetate T=70°C; 4 h;
参考文献
Huesmann, David; Birke, Alexander; Klinker, Kristina; Tuerk, Stephan; Raeder, Hans Joachim; Barz, Matthias
Macromolecules, 2014 , vol. 47, # 3 p. 928 - 936
反应条件
2,6,6-trimethylbicyclo[3.1.1]hept-2-ene in ethyl acetate T=105 - 110°C;
参考文献
Obeid, Rodolphe; Armstrong, Tracy; Peng, Xiaoju; Busse, Karsten; Kressler, Joerg; Scholz, Carmen
Journal of Polymer Science, Part A: Polymer Chemistry, 2014 , vol. 52, # 2 p. 248 - 257
反应条件
in tetrahydrofuran; N,N-dimethyl-formamide T=30°C; 2.5 h; Title compound not separated from byproducts;
参考文献
Blacklock; Shuman; Butcher; Shearin Jr.; Budavari; Grenda
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 836 - 844
反应条件
1: tetrahydrofuran / 2.5 h / 30 °C 2: 88 percent / tetrahydrofuran / 4 h / 25 °C View Scheme
参考文献
Blacklock; Shuman; Butcher; Shearin Jr.; Budavari; Grenda
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 836 - 844
反应条件
in tetrahydrofuran; water T=0 - 12°C; 0.0333333 h;
参考文献
Journal of Organic Chemistry, , vol. 53, # 4 p. 836 - 844
反应条件
1: in tetrahydrofuran
T=-50°C; 3 h;
2: With sodium hydroxide in ethanol; water
20 h; Further stages.;
参考文献
Cherevin; Gulevich; Popova; Zubreichuk; Knizhnikov
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 10 p. 1427 - 1431
