反应条件
in tetrahydrofuran
reaction at -30 - 25°C, later at 50°C, several hours and dehydration of the dihydroxide over P2O5;;
参考文献
Pierce; Levine
Journal of the American Chemical Society, 1953 , vol. 75, p. 1254
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
