3-(二甲基氨基)-1-丙硫醇合成路线 （共 6 条）
反应条件
ethanol; oxygen; iron(II) sulfate
参考文献
Ratschinskii et al.
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 2998,3001,3002;engl.Ausg.S.3027,3028,3030
反应条件
1.1: K2CO3 / acetone / 0.5 h
1.2: acetone
2.1: NaOH / methanol
View Scheme
参考文献
Stanley; Percival; Auer; Braithwaite; Newton; McHale; Hayes
Analytical Chemistry, 2003 , vol. 75, # 7 p. 1573 - 1577
反应条件
sodium hydroxide in methanol
参考文献
Stanley; Percival; Auer; Braithwaite; Newton; McHale; Hayes
Analytical Chemistry, 2003 , vol. 75, # 7 p. 1573 - 1577
反应条件
hydrogen sulfide in isopropyl alcohol
Irradiation;
参考文献
Turk,S.D. et al.
Journal of Organic Chemistry, 1962 , vol. 27, p. 2846 - 2853
反应条件
sodium hydroxide; hydrogen bromide; thiourea
1.) reflux, 72 h, 2.) reflux, 45 min; Multistep reaction;
参考文献
Monteil, Fanny; Queau, Rene; Kalck, Philippe
Journal of Organometallic Chemistry, 1994 , vol. 480, # 1-2 p. 177 - 184
反应条件
water
anschliessenden Behandeln mit wss.Natronlauge;
参考文献
Andrews et al.
Journal of the Chemical Society, 1953 , p. 2998,3000
