1-苯甲酰-1H-苯并三唑合成路线 （共 99 条）
反应条件
aluminium trichloride 1) CH2Cl2, -50 deg C, 30 min, 20 deg C (25 min); 2) CH2Cl2, -50 deg C; Yield given. Multistep reaction;
参考文献
Doklady Chemistry, , vol. 265, p. 291 - 293
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 265, # 6 p. 1406 - 1410
反应条件
1: 2-methyl-3-oxobutanoic acid ethyl ester With sodium hydride in tetrahydrofuran T=20°C; 0.666667 h; 2: PhCOBt in tetrahydrofuran T=20°C;
参考文献
Journal of Organic Chemistry, , vol. 69, # 20 p. 6617 - 6622
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-78 - 20°C; Condensation;
参考文献
Katritzky, Alan R.; Pastor, Alfredo
Journal of Organic Chemistry, 2000 , vol. 65, # 12 p. 3679 - 3681
反应条件
1: in chloroform T=80°C; P=206.859 - 517.148 Torr; 0.166667 h; microwave irradiation; 2: With thionyl chloride in chloroform T=80°C; 0.0333333 h; microwave irradiation;
参考文献
Katritzky, Alan R.; Cai, Chunming; Suzuki, Kazuyuki; Singh, Sandeep K.
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 811 - 814
反应条件
triethylamine in dichloromethane
0.5 h; Ambient temperature;
参考文献
Katritzky, Alan R.; Pastor, Alfredo
Journal of Organic Chemistry, 2000 , vol. 65, # 12 p. 3679 - 3681
反应条件
thionyl chloride in dichloromethane
T=20°C;
参考文献
Katritzky, Alan R.; Cai, Chunming; Singh, Sandeep K.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3375 - 3380
反应条件
palladium diacetate; potassium carbonate in N,N-dimethyl-formamide
T=50°C; P=760 Torr; 10 h;
参考文献
Wang; Chen
Synthetic Communications, 2001 , vol. 31, # 11 p. 1633 - 1637
反应条件
palladium diacetate; potassium carbonate in N,N-dimethyl-formamide
T=50°C; P=760 Torr; 10 h;
参考文献
Wang; Chen
Synthetic Communications, 2001 , vol. 31, # 11 p. 1633 - 1637
反应条件
potassium carbonate in tetrahydrofuran
T=40°C; 57 h;
参考文献
Kim, Jeum-Jong; Park, Yong-Dae; Song Lee, Woo; Cho, Su-Dong; Yoon, Yong-Jin
Synthesis, 2003 , # 10 p. 1517 - 1520
反应条件
triethylamine in tetrahydrofuran
Heating;
参考文献
Katritzky; He; Suzuki
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8210 - 8213
