1-苯甲酰-1H-苯并三唑合成路线 （共 99 条）
反应条件
in benzene
24 h; Irradiation; Mechanism;
参考文献
Parshad; Sharma
Journal of the Indian Chemical Society, 1990 , vol. 67, # 2 p. 150 - 152
反应条件
triethylamine in tetrahydrofuran
T=0 - 20°C; Condensation;
参考文献
Katritzky, Alan R.; Pastor, Alfredo
Journal of Organic Chemistry, 2000 , vol. 65, # 12 p. 3679 - 3681
反应条件
hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
T=20°C; 0.0833333 h;
参考文献
Lin, Shao-Miao; Zhang, Ji-Lei; Chen, Jiu-Xi; Gao, Wen-Xia; Ding, Jin-Chang; Su, Wei-Ke; Wu, Hua-Yue
Journal of the Brazilian Chemical Society, 2010 , vol. 21, # 9 p. 1616 - 1620
反应条件
triethylamine in dichloromethane
T=25°C; 1 h;
参考文献
Katritzky, Alan R.; Shestopalov, Aleksandr A.; Suzuki, Kazuyuki
Synthesis, 2004 , # 11 p. 1806 - 1813
反应条件
triethylamine in N,N-dimethyl-formamide
6 h; Inert atmosphereReflux;
参考文献
Draghici, Bogdan; El-Gendy, Bahaa El-Dien M.; Katritzky, Alan R.
Synthesis, 2012 , vol. 44, # 4 p. 547 - 550
反应条件
samarium; titanium tetrachloride in tetrahydrofuran
24 h; Heating;
参考文献
Wang, Xiaoxia; Zhang, Yongmin
Synthetic Communications, 2003 , vol. 33, # 15 p. 2627 - 2634
反应条件
in chloroform
T=80°C; 0.166667 h; microwave irradiation;
参考文献
Katritzky, Alan R.; Cai, Chunming; Singh, Sandeep K.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3375 - 3380
反应条件
1.1: iPr2NLi / tetrahydrofuran / 1.75 h / -78 °C
1.2: 65 percent / tetrahydrofuran / -78 - 20 °C
2.1: 82 percent / toluene / 0.5 h / Heating
View Scheme
参考文献
Katritzky, Alan R.; Wang, Zuoquan; Wang, Mingyi; Hall, C. Dennis; Suzuki, Kazuyuki
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4854 - 4856
反应条件
1: α-acetylbenzenepropanoic acid ethyl ester With sodium hydride in tetrahydrofuran
T=20°C; 0.666667 h;
2: PhCOBt in tetrahydrofuran
T=20°C; 14 h;
3: With ammonium hydroxide; ammonium chloride in tetrahydrofuran; water
1 h; Heating;
参考文献
Katritzky, Alan R.; Wang, Zuoquan; Wang, Mingyi; Wilkerson, Chavon R.; Hall, C. Dennis; Akhmedov, Novruz G.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6617 - 6622
反应条件
1.1: iPr2NLi / tetrahydrofuran / 1.75 h / -78 °C
1.2: 65 percent / tetrahydrofuran / -78 - 20 °C
2.1: NaH / tetrahydrofuran / 0.67 h / 20 °C
2.2: 51 percent / tetrahydrofuran / 360 h / 20 °C
3.1: 22 percent / toluene / 0.5 h / Heating
View Scheme
参考文献
Katritzky, Alan R.; Wang, Zuoquan; Wang, Mingyi; Hall, C. Dennis; Suzuki, Kazuyuki
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4854 - 4856
