(Z)-1,2-二氯-1-乙氧基乙烯合成路线 (共 63 条)
反应条件
dibenzoyl peroxide in cyclohexane
T=80°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Petrova, R. G.; Churkina, T. D.; Gasanov, R. G.; Lokshin, B. V.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 2 p. 323 - 326
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 2 p. 363 - 367
反应条件
sodium hydroxide; methyllithium; calcium carbonate
und anschliessend reagieren mit Trichloraethylen;
参考文献
Imbert; Konsortium f.elektrochem.Ind.
Patent: DE216940 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 9, p. 25
反应条件
diethyl ether; ethanol
参考文献
Montanari; Negrini
Gazzetta Chimica Italiana, 1957 , vol. 87, p. 1068,1069 Anm. 7
Bollettino Scientifico della Facolta di Chimica Industriale di Bologna, 1956 , vol. 14, p. 68
参考文献
Crompton; Vanderstichele
Journal of the Chemical Society, 1920 , vol. 117, p. 692
Full Text Show Details
Stephens
Journal of the Society of Chemical Industry, London, 1924 , vol. 43, p. 413 T
Chem. Zentralbl., 1925 , vol. 96, # I p. 357
参考文献
Geuther; Brockhoff
Journal fuer Praktische Chemie (Leipzig), 1873 , vol. <2>7, p. 113,115
参考文献
Swarts
Chem. Zentralbl., 1903 , vol. 74, # I p. 13
参考文献
Crompton; Vanderstichele
Journal of the Chemical Society, 1920 , vol. 117, p. 692
反应条件
n-butyllithium
1) a) THF, hexane, -70 deg C, 15 min, b) -10 deg C, 30 min, 2) room temperature, 3 h; Yield given. Multistep reaction;
参考文献
Loffler; Himbert
Synthesis, 1992 , # 5 p. 495 - 498
反应条件
bromine
und Erwaermen oder Aufbewahren des Reaktionsprodukts unter Zutritt von Feuchtigkeit;
参考文献
Crompton; Triffitt
Journal of the Chemical Society, 1921 , vol. 119, p. 1874
反应条件
n-butyllithium; triphenylphosphine; zinc(II) chloride; bis-triphenylphosphine-palladium(II) chloride
1) a) THF, hexane, -70 deg C, 15 min, b) 0 deg C, 5 min, 2) room temperature, 4 h; Yield given. Multistep reaction;
参考文献
Loffler; Himbert
Synthesis, 1992 , # 5 p. 495 - 498