hydrogenchloride; sodium hydroxide in water
1.) 120-140 deg C, 8 h;
参考文献
Shoham, G.; Christianson, D. W.; Bartsch, R. A.; Heo, G. S.; Olsher, U.; Lipscomb, W. N.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1280 - 1285
Hanes, Robert E.; Ellingsworth, Edward C.; Griffin, Scott T.; Rogers, Robin D.; Bartsch, Richard A.
ARKIVOC (Gainesville, FL, United States), 2010 , vol. 2010, # 7 p. 217 - 237,21
1.1: caesium carbonate / acetonitrile / 3 h / 20 °C / |Inert atmosphere; |Reflux
1.2: 24 h / |Inert atmosphere; |Reflux
2.1: 2,4,6-trimethyl-pyridine; lithium iodide / 3 h / 150 °C / |Inert atmosphere
View Scheme
参考文献
Hanes, Robert E.; Ellingsworth, Edward C.; Griffin, Scott T.; Rogers, Robin D.; Bartsch, Richard A.
ARKIVOC (Gainesville, FL, United States), 2010 , vol. 2010, # 7 p. 217 - 237,21
Hanes, Robert E.; Ellingsworth, Edward C.; Griffin, Scott T.; Rogers, Robin D.; Bartsch, Richard A.
ARKIVOC (Gainesville, FL, United States), 2010 , vol. 2010, # 7 p. 217 - 237,21
alkali metals in tetrahydrofuran
various reagents;
参考文献
Rothwell, E. John; Tabner, Brian J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1384 - 1391
Sachleben, Richard A.; Burns, John H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 11 p. 1971 - 1977
