2-氧代-1,2,5,6,7,8-六氢-3-喹啉甲腈合成路线 (共 3 条)
反应条件
1: 48 percent / PBr3 / Heating 2: 59 percent / Zn-dust, acetic acid / ethanol / 0.75 h / Heating View Scheme
参考文献
Paine, John B.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 351 - 355
反应条件
1: With trichlorophosphate
T=20°C; 13 h; Heating / reflux;
2: With sodium hydrogencarbonate in water
参考文献
REDDY US THERAPEUTICS, INC.; BARUAH, Anima; DE, Dibyendu; KHANNA, Ish Kumar; PILLARISETTI, Sivaram; MAITRA, Santanu; ALEXANDER, Christopher, W.; SREENU, Jennepalli; DAGER, Indu
Patent: WO2006/73973 A2, 2006 ;
Location in patent: Page/Page column 244-245 ;
反应条件
phosphorus tribromide
Heating;
参考文献
Paine, John B.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 351 - 355