2-(苯甲酰氧基)-2-苯基乙腈合成路线 （共 69 条）
反应条件
1: trimethylsilyl cyanide; benzaldehyde With 4-(N,N-dimethlyamino)pyridine; vanadium triisopropoxide oxide in acetonitrile
T=25°C; 48 h; Inert atmosphere;
2: acetic anhydride With pyridine in tetrahydrofuran
T=20°C; 24 h;
参考文献
Kodama, Koichi; Kawamata, Hiroaki; Takahashi, Naoya; Hirose, Takuji
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 47 p. 9440 - 9446
反应条件
in dimethyl sulfoxide
T=20°C; 4 h;
参考文献
Katritzky, Alan R.; Abdel-Fattah, Ashraf A.A.; Idzik, Krzysztof R.; El-Gendy, Bahaa El-Dien M.; Soloducho, Jadwiga
Tetrahedron, 2007 , vol. 63, # 28 p. 6477 - 6484
反应条件
tris(pentafluorophenyl)-borane
T=20°C; 5 h; Neat (no solvent);
参考文献
Kadam, Santosh T.; Kim, Sung Soo
Tetrahedron, 2009 , vol. 65, # 32 p. 6330 - 6334
反应条件
sodium tetrahydroborate; tetrabutylammomium bromide in dichloromethane; water
参考文献
Photis, James M.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 182 - 184
反应条件
18-crown-6 ether in dichloromethane
Ambient temperature;
参考文献
Chenevert, Robert; Plante, Raymond; Voyer, Normand
Synthetic Communications, 1983 , vol. 13, # 5 p. 403 - 410
反应条件
4-(N,N-dimethlyamino)pyridine; oxygen; vanadium triisopropoxide oxide in acetonitrile
T=25°C; 48 h;
参考文献
Kodama, Koichi; Kawamata, Hiroaki; Takahashi, Naoya; Hirose, Takuji
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 47 p. 9440 - 9446
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile
T=20°C; 12 h;
参考文献
Poisson, Thomas; Dalla, Vincent; Papamicael, Cyril; Dupas, Georges; Marsais, Francis; Levacher, Vincent
Synlett, 2007 , # 3 p. 381 - 386
反应条件
sodium hydride in N,N-dimethyl-formamide
0.5 h;
参考文献
Miyashita; Sato; Taido; Tanji; Oishi; Higashino
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 1 p. 230 - 233
反应条件
in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Yoneda, Ryuji; Santo, Kazunori; Harusawa, Shinya; Kurihara, Takushi
Synthesis, 1986 , # 12 p. 1054 - 1055
反应条件
sodium hydride in tetrahydrofuran
0.5 h; Heating;
参考文献
Tanji; Sato; Kanamura; Iijima; Miyashita; Higashino
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 2 p. 513 - 517
