N-叔丁基-4-甲基苯甲酰胺合成路线 （共 18 条）
反应条件
water; caesium carbonate in acetone
T=0°C; 0.333333 h; Schlenk techniqueInert atmosphere;
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113
反应条件
dicobalt octacarbonyl in benzene
T=180°C; P=56886.3 - 67229.2 Torr; stainless steel autoclave;
参考文献
Antebi, Shlomo; Alper, Howard
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2010 - 2012
反应条件
4-(N,N-dimethlyamino)pyridine; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane
T=160°C; 0.333333 h; Microwave irradiation;
参考文献
Odell, Luke R.; Saevmarker, Jonas; Larhed, Mats
Tetrahedron Letters, 2008 , vol. 49, # 42 p. 6115 - 6118
反应条件
potassium fluoride; 18-crown-6 ether; water in tetrahydrofuran
T=30°C; 16 h; Inert atmosphere; Overall yield = 59 percent; Overall yield = 0.056 g; regioselective reaction;
参考文献
Kaicharla, Trinadh; Thangaraj, Manikandan; Biju, Akkattu T.
Organic Letters, 2014 , vol. 16, # 6 p. 1728 - 1731
反应条件
1: hydrofluoroboric acid; sodium nitrite / water / 0.58 h / 0 °C
2: caesium carbonate; water / acetone / 0.33 h / 0 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113
反应条件
1: 93 percent / Et3N / diethyl ether / 2 h / 20 °C
2: 1.) t-BuOK, 2.) aq. NH4Cl / 1.) THF, reflux, 2 h
View Scheme
参考文献
Aitken, R. Alan; Raut, Swati V.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 7 p. 747 - 751
反应条件
NaOD; potassium chloride; water-d2
T=100°C; Rate constant;
参考文献
Slebocka-Tilk; Bennet; Keillor; Brown; Guthrie, J. Peter; Jodhan
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8507 - 8514
反应条件
TPPBr2; triethylamine in chloroform
T=-60 - 20°C; von Braun degradation;
参考文献
Vaccari, Daniele; Davoli, Paolo; Spaggiari, Alberto; Prati, Fabio
Synlett, 2008 , # 9 p. 1317 - 1320
