(4-甲基-吡啶-2-基)-甲醇合成路线 (共 14 条)
反应条件
(NH4)2S2O8
1 h; Heating; Yield given;
参考文献
Katz, R B; Mistry, J; Mitchell, M B
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 317 - 326
反应条件
anschliessend Erhitzen mit wss. Salzsaeure;
参考文献
Furukawa
Pharmaceutical Bulletin, 1955 , vol. 3, p. 413,415
Yakugaku Zasshi, 1956 , vol. 76, p. 900
Chem.Abstr., 1957 , p. 2770
反应条件
thionyl chloride in dichloromethane
Inert atmosphere;
参考文献
Prat, Irene; Font, David; Company, Anna; Junge, Kathrin; Ribas, Xavi; Beller, Matthias; Costas, Miquel
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 5 p. 947 - 956
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane
T=0°C; 0.333333 h;
参考文献
TRIGEN LIMITED
Patent: WO2005/12323 A2, 2005 ;
Location in patent: Page/Page column 42 ;
WO 2005/012323 A2