2,6-二氯吡啶-4-羰酰氯合成路线 （共 22 条）
反应条件
phosphorus pentachloride
参考文献
Wibaut; Overhoff
Recueil des Travaux Chimiques des Pays-Bas, 1933 , vol. 52, p. 55,59
反应条件
anhydrous tetramethylammonium chloride; trichlorophosphate T=130°C; 18 h;
参考文献
The Regents of the University Of California
Patent: WO2004/46103 A2, 2004 ;
Location in patent: Page 33-34 ;
反应条件
1: 100 percent / lithium hydroxide / tetrahydrofuran; H2O / 1.5 h / 20 °C 2: oxalyl chloride / tetrahydrofuran; CH2Cl2 / 4 h View Scheme
参考文献
MacIejewski, John P.; Wipf, Peter
Arkivoc, 2011 , vol. 2011, # 6 p. 92 - 119
参考文献
Sell; Dootson
Journal of the Chemical Society, 1897 , vol. 71, p. 1082
Journal of the Chemical Society, 1898 , vol. 73, p. 441
Full Text Show Details
Behrmann; Hofmann
Chemische Berichte, 1884 , vol. 17, p. 2689
参考文献
Sell; Dootson
Journal of the Chemical Society, 1897 , vol. 71, p. 1082
Journal of the Chemical Society, 1898 , vol. 73, p. 441
反应条件
sodium hydroxide in ethylene glycol dimethyl ether; dichloromethane; water T=20°C; 1.5 h;
参考文献
ANALYTECON S.A.
Patent: WO2005/87743 A1, 2005 ;
Location in patent: Page/Page column 36 ;
WO 2005/087743 A1
反应条件
1: sodium azide / water; acetone / 0.03 h / 25 °C 2: trifluoroacetic acid / benzene / 21 h / 90 °C 3: potassium carbonate / methanol / 7.5 h / 25 °C 4: sulfuric acid; nitric acid / -5 °C View Scheme
参考文献
Ehmke, Veronika; Winkler, Edwin; Banner, David W.; Haap, Wolfgang; Schweizer, W. Bernd; Rottmann, Matthias; Kaiser, Marcel; Freymond, Celine; Schirmeister, Tanja; Diederich, Francois
ChemMedChem, 2013 , vol. 8, # 6 p. 967 - 975
反应条件
2: thionyl chloride / 120 °C / im Rohr View Scheme
参考文献
Wibaut; Overhoff
Recueil des Travaux Chimiques des Pays-Bas, 1933 , vol. 52, p. 55,59
反应条件
1: sodium azide / water; acetone / 0.03 h / 25 °C 2: trifluoroacetic acid / benzene / 21 h / 90 °C 3: potassium carbonate / methanol / 7.5 h / 25 °C 4: sulfuric acid; nitric acid / -5 °C 5: sulfuric acid / 1 h / 0 - 100 °C View Scheme
参考文献
Ehmke, Veronika; Winkler, Edwin; Banner, David W.; Haap, Wolfgang; Schweizer, W. Bernd; Rottmann, Matthias; Kaiser, Marcel; Freymond, Celine; Schirmeister, Tanja; Diederich, Francois
ChemMedChem, 2013 , vol. 8, # 6 p. 967 - 975
反应条件
2: P2O5 / unter vermindertem Druck 3: SnCl2; HCl; diethyl ether View Scheme
参考文献
Wibaut; Overhoff
Recueil des Travaux Chimiques des Pays-Bas, 1933 , vol. 52, p. 55,59
