2,7-二羟基-9-芴酮合成路线 （共 24 条）
反应条件
zinc(II) chloride T=210°C; Neat (no solvent);
参考文献
Roxin, Aron; Chase, Alex; Jeffers, Elizabeth; Lukeman, Matthew
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 6 p. 920 - 930
反应条件
potassium hydroxide 2 h; Heating;
参考文献
Lio, Jingdong; Haller, Marnie; Li, Hongxiang; Tang, Hong-Zhi; Jen, Alex K.-Y.; Jakka, Kavitha; Chou, Chia-Hung; Shu, Ching-Fong
Macromolecules, 2004 , vol. 37, # 2 p. 248 - 250
反应条件
1: sodium carbonate / tris(dibenzylideneacetone)dipalladium(0) / 1,2-dimethoxy-ethane; H2O / 85 °C 2: sodium hydroxide / ethanol / 78 °C 3: thionyl chloride / 79 °C View Scheme
参考文献
Epperson, James R.; Bruce, Marc A.; Catt, John D.; Deskus, Jeffrey A.; Hodges, Donald B.; Karageorge, George N.; Keavy, Daniel J.; Mahle, Cathy D.; Mattson, Ronald J.; Ortiz, Astrid A.; Parker, Michael F.; Takaki, Katherine S.; Watson, Brett T.; Yevich, Joseph P.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 17 p. 4601 - 4611
反应条件
1: sodium carbonate / tris(dibenzylideneacetone)dipalladium(0) / 1,2-dimethoxy-ethane; H2O / 85 °C 2: sodium hydroxide / ethanol / 78 °C 3: thionyl chloride / 79 °C View Scheme
参考文献
Epperson, James R.; Bruce, Marc A.; Catt, John D.; Deskus, Jeffrey A.; Hodges, Donald B.; Karageorge, George N.; Keavy, Daniel J.; Mahle, Cathy D.; Mattson, Ronald J.; Ortiz, Astrid A.; Parker, Michael F.; Takaki, Katherine S.; Watson, Brett T.; Yevich, Joseph P.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 17 p. 4601 - 4611
反应条件
1: sodium hydroxide / ethanol / 78 °C 2: thionyl chloride / 79 °C View Scheme
参考文献
Epperson, James R.; Bruce, Marc A.; Catt, John D.; Deskus, Jeffrey A.; Hodges, Donald B.; Karageorge, George N.; Keavy, Daniel J.; Mahle, Cathy D.; Mattson, Ronald J.; Ortiz, Astrid A.; Parker, Michael F.; Takaki, Katherine S.; Watson, Brett T.; Yevich, Joseph P.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 17 p. 4601 - 4611
反应条件
1: With AlCl3, aluminium chloride; acetic anhydride 2: With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid in chloroform Further stages;
参考文献
Roxin, Aron; Chase, Alex; Jeffers, Elizabeth; Lukeman, Matthew
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 6 p. 920 - 930
反应条件
hydrogen bromide in acetic acid
参考文献
Horner,L.; Baston,D.W.
Justus Liebigs Annalen der Chemie, 1973 , p. 910 - 935
反应条件
1: 87 percent / AlCl3 / benzene / Heating 2: CaO / melting View Scheme
参考文献
Oleinik, A. F.; Adamskaya, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 11 p. 1221 - 1224
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 11 p. 1537 - 1539
反应条件
1: 66 percent 2: 87 percent / AlCl3 / benzene / Heating 3: CaO / melting View Scheme
参考文献
Oleinik, A. F.; Adamskaya, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 11 p. 1221 - 1224
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 11 p. 1537 - 1539
反应条件
1: (i) Cu, (ii) aq. NaOH, MeOH 2: polyphosphoric acid 3: aq. HBr / acetic acid View Scheme
参考文献
Horner,L.; Baston,D.W.
Justus Liebigs Annalen der Chemie, 1973 , p. 910 - 935
