2,7-二羟基-9-芴酮合成路线 （共 24 条）
反应条件
1: (i) Cu, (ii) aq. NaOH, MeOH 2: polyphosphoric acid 3: aq. HBr / acetic acid View Scheme
参考文献
Horner,L.; Baston,D.W.
Justus Liebigs Annalen der Chemie, 1973 , p. 910 - 935
反应条件
1: polyphosphoric acid 2: aq. HBr / acetic acid View Scheme
参考文献
Horner,L.; Baston,D.W.
Justus Liebigs Annalen der Chemie, 1973 , p. 910 - 935
反应条件
1: potassium permanganate / water / Heating 2: sodium hydroxide 3: zinc(II) chloride / 210 °C / Neat (no solvent) View Scheme
参考文献
Roxin, Aron; Chase, Alex; Jeffers, Elizabeth; Lukeman, Matthew
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 6 p. 920 - 930
反应条件
1: (i) SnCl2, HCl, AcOH, (ii) NaOH 2: aq. HBF4, NaNO2 3: aq. H2SO4 View Scheme
参考文献
Burke,S.M.; Joullie,M.M.
Synthetic Communications, 1976 , vol. 6, p. 371 - 376
反应条件
1: aq. HBF4, NaNO2 2: aq. H2SO4 View Scheme
参考文献
Burke,S.M.; Joullie,M.M.
Synthetic Communications, 1976 , vol. 6, p. 371 - 376
参考文献
Oleinik, A. F.; Adamskaya, E. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 11 p. 1221 - 1224
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 11 p. 1537 - 1539
反应条件
1: 2,7-dihydroxy-9H-fluoren-9-one With potassium carbonate; sodium iodide in N,N-dimethyl-formamide T=80°C; 1 h; 2: 2-(2-hydroxyethoxy)ethyl chloride in N,N-dimethyl-formamide T=80°C; 35 h;
参考文献
Lukyanenko, Nikolay G.; Kirichenko, Tatiana I.; Lyapunov, Alexander Yu.; Kulygina, Catherine Yu.; Simonov, Yurii A.; Fonari, Marina S.; Botoshansky, Mark M.
Tetrahedron Letters, 2004 , vol. 45, # 14 p. 2927 - 2930
反应条件
potassium carbonate in acetone Heating;
参考文献
Ivanov; Lyakhov; Yarkova; Galatina; Mazepa
Russian Journal of General Chemistry, 2002 , vol. 72, # 9 p. 1435 - 1438
反应条件
potassium hydroxide in toluene
参考文献
Burke,S.M.; Joullie,M.M.
Synthetic Communications, 1976 , vol. 6, p. 371 - 376
反应条件
potassium carbonate in N,N-dimethyl-formamide 0.5 h; Heating;
参考文献
Litvinova, L. A.; Lyakhov, S. A.; Zhukova, N. A.; Andronati, S. A.; Musienko, V. I.; et al.
Pharmaceutical Chemistry Journal, 1989 , vol. 23, # 6 p. 497 - 499
Khimiko-Farmatsevticheskii Zhurnal, 1989 , vol. 23, # 6 p. 702 - 704
