反应条件
in 1,2-dichloro-ethane addn.of PhNCS to a soln. of the Sn-compound under N2; stirred at 40°C for 2 h; solvent was removed in vac.; column chromy. (silica gel; eluent: C6H6); vac. distn. (120°C/0.1 Torr);
参考文献
Yano, Katsunori; Baba, Akio; Matsuda, Haruo
Chemische Berichte, 1991 , vol. 124, # 8 p. 1881 - 1884
