反应条件
in hexane byproducts: ((CH3)2CHS)2, (CH3)2CHBr, (CH3)2CHSH; Ti complex suspended in hexanes, addn. of Br2, stirred (15 min.); ppt. collected on a filter in air, dried (Cp2TiBr2 and Cp2Ti(SCHMe2)Br, detected by NMR); removal of solvent from the filtrate (mostly disulfide, minute amts. of the monosulfides and bromide, GC anal.);
参考文献
Shaver, Alan; Morris, Stephen; Desjardin, Alain
Inorganica Chimica Acta, 1989 , vol. 161, p. 11 - 12
