(S)-(+)-1,2-丙二醇合成路线 （共 56 条）
反应条件
lithium aluminium tetrahydride in diethyl ether 0.5 h; Heating;
参考文献
Licandro, Emanuela; Maiorana, Stefano; Manzotti, Raffaella; Papagni, Antonio; Pryce, Mary; et al.
Gazzetta Chimica Italiana, 1997 , vol. 127, # 12 p. 815 - 818
反应条件
silica gel supported sodium hydrogen sulfate in methanol; dichloromethane T=20°C;
参考文献
Petursson, Sigthor; Jonsdottir, Sigridur
Tetrahedron Asymmetry, 2011 , vol. 22, # 18-19 p. 1809 - 1812
反应条件
hydrogen; RuBr2[(S)-(C6H2OCH2CH2OP(C6H5)2)2] in methanol T=80°C; P=22501.8 Torr; 40 h;
参考文献
Jeulin, Severine; Champion, Nicolas; Dellis, Philippe; Ratovelomanana-Vidal, Virginie; Genet, Jean-Pierre
Synthesis, 2005 , # 20 art. no. Z17405SS, p. 3666 - 3671
反应条件
lithium aluminium tetrahydride in diethyl ether T=0 - 20°C; 2.25 h;
参考文献
Tsotinis, Andrew; Calogeropoulou, Theodora; Koufaki, Maria; Souli, Charikleia; Balzarini, Jan; De Clercq, Erik; Makriyannis, Alexandros
Journal of Medicinal Chemistry, 1996 , vol. 39, # 17 p. 3418 - 3422
反应条件
in water T=30°C; 48 h; sucrose, Baker's yeast; Title compound not separated from byproducts;
参考文献
Thanos, Iordanes; Simon, Helmut
Angewandte Chemie, 1986 , vol. 98, # 5 p. 455 - 456
反应条件
palladium 10 on activated carbon; hydrogen in methanol
参考文献
Petursson, Sigthor; Jonsdottir, Sigridur
Tetrahedron Asymmetry, 2012 , vol. 23, # 2 p. 157 - 163
反应条件
hydrogen; dihydridotetrakis(triphenylphosphine)ruthenium(II); 1,1,1-tris (diphenylphosphinomethyl)ethane in methanol T=80°C; P=37503.8 Torr; 13 h; Inert atmosphereAutoclave;
参考文献
Takasago International Corporation
Patent: EP2141142 A1, 2010 ;
Location in patent: Page/Page column 17 ;
反应条件
[RuH(CO)(BPy-tPNN*)]; hydrogen in tetrahydrofuran T=110°C; P=38002.6 Torr; 12 h; Inert atmosphere;
参考文献
Balaraman, Ekambaram; Fogler, Eran; Milstein, David
Chemical Communications, 2012 , vol. 48, # 8 p. 1111 - 1113
反应条件
[(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(III) acetate; water T=0 - 20°C; 12 h;
参考文献
Berkessel, Albrecht; Ertuerk, Erkan
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 18 p. 2619 - 2625
反应条件
cobalt, [[2,2'-[(1R,2R)-1,2-cyclohexanediylbis[(nitrilo-κN)methylidyne]]bis[4,6-bis(1,1dimethylethyl)phenolato-κO]](2-)]-, (SP-4-2)-; water; acetic acid in toluene T=0 - 20°C;
参考文献
Bates, Roderick W.; Lu, Yongna
Organic Letters, 2010 , vol. 12, # 17 p. 3938 - 3941
