(S)-(+)-1,2-丙二醇合成路线 (共 56 条)
反应条件
hydrogen; palladium on activated charcoal in methanol 30 h;
参考文献
Manzocchi, Ada; Fiecchi, Alberto; Santaniello, Enzo
Synthesis, 1987 , # 11 p. 1007 - 1009
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water T=20°C; 14 h;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
hydrogen; ruthenium on silica in dimethyl-ether T=150°C; 0.666667 h; Product distribution / selectivity;
参考文献
AVECIA LIMITED
Patent: WO2005/23737 A1, 2005 ;
Location in patent: Page/Page column 12-13 ;
反应条件
hydrogenchloride in methanol 12 h;
参考文献
Cooper, Keith D.; Walborsky, Harry M.
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2110 - 2116
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in ethanol 1 h;
参考文献
Kobayashi; Takase; Ito; Terashima
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 9 p. 3038 - 3040
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in ethanol 1 h;
参考文献
Kobayashi; Takase; Ito; Terashima
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 9 p. 3038 - 3040
反应条件
1: With titanium(IV) isopropylate; (-)-(R,R)-TADDOL in diphenylether T=90°C; 1 h; 2: Propylene glycol in diphenylether T=90°C; 0.166667 h; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2009/30235 A1, 2009 ;
Location in patent: Page/Page column 14 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Sugawara, Fumio; Nakayama, Haruhiko; Stroebel, Gary A.; Ogawa, Tomoya
Agricultural and Biological Chemistry, 1986 , vol. 50, # 9 p. 2261 - 2272
反应条件
water; chiral ((substituted salen)Co)2-InCl3 T=20°C; 2 h;
参考文献
Thakur, Santosh Singh; Chen, Shu-Wei; Li, Wenji; Shin, Chang-Kyo; Koo, Yoon-Mo; Kim, Geon-Joong
Synthetic Communications, 2006 , vol. 36, # 16 p. 2371 - 2383
反应条件
1: With titanium(IV) isopropylate; 1-dodecylamine; (-)-(R,R)-TADDOL in diphenylether T=90°C; 1 h; 2: Propylene glycol in diphenylether T=90°C; 0.166667 h; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2009/30235 A1, 2009 ;
Location in patent: Page/Page column 14 ;