2-溴-4'-苄氧基苯乙酮合成路线 （共 13 条）
反应条件
hydrogenchloride; bromine in methanol T=0 - 20°C;
参考文献
Goswami, Jonalee; Goswami, Amrit
Journal of the Indian Chemical Society, 2002 , vol. 79, # 5 p. 469 - 471
反应条件
bromine; aluminium trichloride in tetrahydrofuran; hexane; chloroform; water; benzene
参考文献
Mitsubishi Kasei Corporation
Patent: US4933344 A1, 1990 ;
反应条件
in chloroform; ethyl acetate
参考文献
Novartis AG
Patent: US6051577 A1, 2000 ;
US 6051577 A
反应条件
1: KOH; tetraethylammonium iodide / acetonitrile / Heating 2: 90 percent / Br2; conc. aq. HCl / methanol / 0 - 20 °C View Scheme
参考文献
Cao, Banpeng; Ding, Haixin; Yang, Ruchun; Wang, Xiaoji; Xiao, Qiang
Marine Drugs, 2012 , vol. 10, # 6 p. 1412 - 1421
反应条件
copper(ll) bromide in chloroform; ethyl acetate 5 h; Reflux;
参考文献
Roman, Gheorghe; Vlahakis, Jason Z.; Vukomanovic, Dragic; Nakatsu, Kanji; Szarek, Walter A.
ChemMedChem, 2010 , vol. 5, # 9 p. 1541 - 1555
反应条件
1: potassium carbonate / acetone / 0 °C 2: phenyltrimethylammonium tribromide / tetrahydrofuran / 20 °C View Scheme
参考文献
Cao, Banpeng; Ding, Haixin; Yang, Ruchun; Wang, Xiaoji; Xiao, Qiang
Marine Drugs, 2012 , vol. 10, # 6 p. 1412 - 1421
反应条件
1: KOH; tetraethylammonium iodide / acetonitrile / Heating 2: 90 percent / Br2; conc. aq. HCl / methanol / 0 - 20 °C View Scheme
参考文献
Reznikov,V.M.; Novitskii,V.F.
Chemistry of Natural Compounds, 1975 , vol. 11, p. 71 - 75
Khimiya Prirodnykh Soedinenii, 1975 , vol. 11, # 1 p. 73 - 77
反应条件
1: sodium azide / tetrabutylammomium bromide / dichloromethane; water / 4 h / 20 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 2.33 h / 0 - 20 °C View Scheme
参考文献
ABBOTT HEALTHCARE PRODUCTS B.V.; IWEMA BAKKER, Wouter, I.; COOLEN, Hein K.A.C.; MONS, Harmen; STOIT, Axel; RONKEN, Eric; KAM, VAN DER, Elizabeth; FRANKENA, Jurjen
Patent: WO2011/23795 A1, 2011 ;
WO 2011/023795 A1
反应条件
C31H33ClN2O8RhS3(2-)*2Na(1+); sodium formate in water T=40°C; 1 h; Inert atmosphere; enantioselective reaction;
参考文献
RSC Advances, , vol. 3, # 6 p. 1825 - 1834
反应条件
sodium formate; N-hexadecyl-N,N,N-trimethylammonium bromide; sodium lauryl sulfate; (R,R)-TsDPEN; [{(η5-C5Me5)RhCl}2(μ-Cl)2] in water T=28°C; 2 h; Title compound not separated from byproducts;
参考文献
Wang, Fei; Liu, Hui; Cun, Linfeng; Zhu, Jin; Deng, Jingen; Jiang, Yaozhong
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9424 - 9429
