反应条件
1: 71 percent / diethyl ether / 2 h / Ambient temperature
2: 74 percent / lithium amide, ammonia / tetrahydrofuran / 4 h / Ambient temperature
3: 1) CrO3, pyridine / 1) CH2Cl2, 15-20 deg C, 0.5 h; 2) 15 min
4: 5.05 g / triethylamine, H2 / palladium/calcium carbonate / tetrahydrofuran
5: Jones reagent / acetone / 2 h / Ambient temperature
View Scheme
参考文献
Joshi, N. N.; Bhandari, R. G.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 8 p. 698 - 701
