2-(4-甲氧苯基)噻吩合成路线 （共 72 条）
反应条件
1-methyl-pyrrolidin-2-one; copper(l) iodide; 2-tri(n-butyl)stannylthiophene; cesium fluoride T=90°C; 7 h; other reagents: 2-thienyltributylstannane/CuI/KF, 2-thienyltributylstannane/MnBr2/KF, 2-thienyltributylstannane/MnBr2/LiCl, 2-thienyltributylstannane/MnBr2/CsF;
参考文献
Kang, Suk-Ku; Kim, Jae-Sun; Choi, Sang-Chul
Journal of Organic Chemistry, 1997 , vol. 62, # 13 p. 4208 - 4209
反应条件
1: 87 percent / DMAP; DCC / CH2Cl2 / 17 h / 20 °C 2: 11 percent / Lawesson's reagent / 0.05 h / MW irradiation View Scheme
参考文献
Kiryanov; Sampson; Seed
Journal of Organic Chemistry, 2001 , vol. 66, # 23 p. 7925 - 7929
反应条件
manganese triacetate Heating;
参考文献
Demir, Ayhan S.; Reis, Oemer; Emrullahoglu, Mustafa
Tetrahedron, 2002 , vol. 58, # 40 p. 8055 - 8058
反应条件
aluminium trichloride in dichloromethane 0 deg C, 30 min; r.t., 60 min; reflux, 30 min; Further byproducts given;
参考文献
Sone, Tyo; Yokoyama, Ryoji; Okuyama, Yohko; Sato, Kazuaki
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 83 - 88
反应条件
aluminium trichloride in dichloromethane 0 deg C, 30 min; r.t., 60 min; reflux, 30 min; Further byproducts given;
参考文献
Sone, Tyo; Yokoyama, Ryoji; Okuyama, Yohko; Sato, Kazuaki
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 83 - 88
反应条件
18-crown-6 ether; potassium acetate
参考文献
Ellames, George J; Gibson, Jennifer S; Herbert, John M; McNeill, Alan H
Tetrahedron, 2001 , vol. 57, # 46 p. 9487 - 9497
反应条件
1-methyl-pyrrolidin-2-one; potassium fluoride; copper(l) iodide T=90°C; 7 h; other organostannanes, other organic iodides, other reagents: CuI/NaCl, CuI/KCl, CuI/LiCl, CuI/CsF, MnBr2/NaCl, MnBr2/KCl, MnBr2/KF, MnBr2/LiCl, MnBr2/CsF, MnCl2*4H2O, MnI2, DMF presence, other temperature and time; Product distributionMechanism;
参考文献
Kang, Suk-Ku; Kim, Jae-Sun; Choi, Sang-Chul
Journal of Organic Chemistry, 1997 , vol. 62, # 13 p. 4208 - 4209
反应条件
in water; acetonitrile Photolysis; Product distribution; Further Variations:Solvents;
参考文献
Manet, Ilse; Monti, Sandra; Grabner, Gottfried; Protti, Stefano; Dondi, Daniele; Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Chemistry - A European Journal, 2008 , vol. 14, # 3 p. 1029 - 1039
反应条件
in water; acetonitrile Photolysis; Product distribution; Further Variations:Solvents;
参考文献
Manet, Ilse; Monti, Sandra; Grabner, Gottfried; Protti, Stefano; Dondi, Daniele; Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Chemistry - A European Journal, 2008 , vol. 14, # 3 p. 1029 - 1039
反应条件
n-butyllithium 1) THF, 0 deg C, 1h, 2) r.t., 16 h; Yield given. Multistep reaction;
参考文献
Mignani; Leising; Meyrueix; Samson
Tetrahedron Letters, 1990 , vol. 31, # 33 p. 4743 - 4746
