反应条件
catalyst: Pd(OAc)2-triphenylphosphine in dimethyl sulfoxide
under Ar; DMSO, CH2CHCH2Cl, allylstannane, NCCH2CO2CH3 added to mixt. ofPd(OAc)2 and PPh3 (molar ratio 8:7:4:1:2); heated at 100°C for 2 0 h; treated with water; extd. with ether; distd. under reduced pressure; detd. by GC;
参考文献
Kiji, Jitsuo; Okano, Tamon; Nomura, Takaaki; Saiki, Kayoko; Sai, Torei; Tsuji, Jiro
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 10 p. 1939 - 1945