2-(1-羟基戊基)-1-环戊酮合成路线 （共 11 条）
反应条件
H3PO4/C; hydrogen; 5 palladium on charcoal T=140°C; P=757.576 Torr; 20 h;
参考文献
Kao Corporation
Patent: EP2487150 A1, 2012 ;
Location in patent: Page/Page column 10 ;
反应条件
hydrogen; 5 Pd(II)/C(eggshell); H3PO4/C T=140°C; P=757.576 Torr; 10 h; Inert atmosphere; Product distribution / selectivity;
参考文献
KAO CORPORATION
Patent: US2011/34722 A1, 2011 ;
Location in patent: Page/Page column 8; 9 ;
反应条件
1: With oxalic acid T=120°C; 2: With hydrogenchloride; 3-Methylpyridine in water; butan-1-ol T=130°C; 4 h;
参考文献
KAO CORPORATION
Patent: EP1433773 A1, 2004 ;
Location in patent: Page 11 ;
参考文献
Kao Corporation
Patent: EP2266943 A1, 2010 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen; 5 Pd(II)/C(eggshell); H3PO4/C T=140°C; P=757.576 Torr; 10 h; Inert atmosphere; Product distribution / selectivity;
参考文献
KAO CORPORATION
Patent: US2011/34722 A1, 2011 ;
Location in patent: Page/Page column 8; 9 ;
反应条件
1: hydrogen / 5 Pd(II)/C(eggshell); H3PO4/C / 10 h / 140 °C / 757.58 Torr / Inert atmosphere 2: sodium methylate / methanol / 0 °C / Inert atmosphere 3: water / 4 h / 215 °C View Scheme
参考文献
KAO CORPORATION
Patent: US2011/34722 A1, 2011 ;
反应条件
Titanium(IV) oxide T=100°C; P=397.54 Torr;
参考文献
Kao Corporation
Patent: EP2269971 A1, 2011 ;
Location in patent: Page/Page column 7 ;
反应条件
1: With sodium hydroxide in water
T=15°C; 9 h;
2: With sodium hydroxide
2 h;
参考文献
KAO CORPORATION
Patent: EP1433773 A1, 2004 ;
Location in patent: Page 7 ;
反应条件
1: With sodium hydroxide in water
T=5 - 15°C; 6 - 8 h;
2: With phosphoric acid in water
Product distribution / selectivity;
参考文献
KAO CORPORATION
Patent: EP1577287 A2, 2005 ;
Location in patent: Page/Page column 6-9 ;
参考文献
Lardelli,G. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1967 , vol. 86, p. 481 - 503
