反应条件
1.1: dichloromethane / 20 h / |Reflux; |Large scale
2.1: pyridine / ethyl acetate / 1 h / 20 °C / |Large scale
3.1: camphor-10-sulfonic acid / ethyl acetate / 6 h / |Reflux; |Large scale
3.2: Amberlyst-15 resin / 1 h / |Reflux; |Large scale
4.1: sodium hydroxide / toluene; water / 5 h / 20 °C
View Scheme
参考文献
Braden, Timothy M.; Coffey, D. Scott; Doecke, Christopher W.; LeTourneau, Michael E.; Martinelli, Michael J.; Meyer, Christopher L.; Miller, Richard D.; Pawlak, Joseph M.; Pedersen, Steven W.; Schmid, Christopher R.; Shaw, Bruce W.; Staszak, Michael A.; Vicenzi, Jeffrey T.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 431 - 440
