2-甲基-3-乙氧基丙烯醛合成路线 （共 18 条）
反应条件
water; toluene-4-sulfonic acid
参考文献
Klimko,V.T. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1962 , vol. 32, p. 2961 - 2966,2913 - 2918
反应条件
trichlorophosphate 1.) <30 deg C, 2.) 70 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nair,V.; Vietti,D.E.; Cooper,C.S.
Journal of the American Chemical Society, 1981 , vol. 103, p. 3030
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Sydnes, Leiv K.; Bakstad, Einar
Acta Chemica Scandinavica, 1996 , vol. 50, # 5 p. 446 - 453
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Sydnes, Leiv K.; Bakstad, Einar
Acta Chemica Scandinavica, 1996 , vol. 50, # 5 p. 446 - 453
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Sydnes, Leiv K.; Bakstad, Einar
Acta Chemica Scandinavica, 1996 , vol. 50, # 5 p. 446 - 453
反应条件
ion-exchange resin lt;H+ formgt;
参考文献
Stavrovskaya,A.V. et al.
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, p. 1194 - 1198,1148 - 1151
反应条件
hydrogenchloride; potassium hydroxide 1) 80 deg C, 1 h; Multistep reaction;
参考文献
Ullrich, Friedrich-Wilhelm; Rotscheidt, Klaus; Breitmaier, Eberhard
Chemische Berichte, 1986 , vol. 119, # 5 p. 1737 - 1744
反应条件
sodium methylate 1) CH3OH, THF, 25 deg C, 4 h and 5 min, 2) DMF, 40 deg C (bath temperature), 20 h; Yield given. Multistep reaction;
参考文献
Babler, James H.; Liptak, Vincent P.; Trautmann, Jeffrey A.; Zayia, Gregory H.
Synthetic Communications, 1996 , vol. 26, # 10 p. 1943 - 1951
反应条件
sodium ethanolate in ethanol 24 h; Heating;
参考文献
Shaw; Shetlar
Journal of the American Chemical Society, 1990 , vol. 112, # 21 p. 7736 - 7742
参考文献
Breitmaier,E.; Gassenmann,S.
Chemische Berichte, 1971 , vol. 104, p. 665 - 667
