5-苯基-4-戊烯-2-酮合成路线 (共 29 条)
反应条件
lithium chloride; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
T=23°C; 20 h;
参考文献
Valle, L. Del; Stille, J. K.; Hegedus, L. S.
Journal of Organic Chemistry, 1990 , vol. 55, p. 3019 - 3023
反应条件
2,6-dichloropyridine-N-oxide; Ru(IV)(TDCPP)Cl2 in chloroform-d1
T=60°C; 6 h;
参考文献
Chen, Jian; Che, Chi-Ming
Angewandte Chemie - International Edition, 2004 , vol. 43, # 37 p. 4950 - 4954
反应条件
[RuIV(meso-tetrakis(2,6-dichlorophenyl)porphyrin)Cl2]; 2,6-dichloropyridine-N-oxide in chloroform-d1
T=60°C; Wacker Oxidation; 6 h;
参考文献
Wang, Zhi-Ming; Sang, Xue-Ling; Che, Chi-Ming; Chen, Jian
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1736 - 1739
反应条件
boron trifluoride diethyl etherate in chloroform
T=0°C; 0.25 h;
参考文献
Sato, Tadashi; Kikuchi, Toshihiro; Tsujita, Hiroshi; Kaetsu, Atsushi; Sootome, Norio; Nishida, Ken-Ichiro; Tachibana, Kazutaka; Murayama, Eigoro
Tetrahedron, 1991 , vol. 47, # 20-21 p. 3281 - 3304
反应条件
pyridine; chromium(VI) oxide in dichloromethane
3 h;
参考文献
Bowers, Kevin G.; Mann, John; Walsh, E. Brian; Howarth, Oliver W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1657 - 1666
反应条件
tetra-n-butylammonium tetrafluoroborate; NiBr2bipy in N,N-dimethyl-formamide
T=60°C; electroreductive coupling; Electrochemical reaction;
参考文献
Cannes; Condon; Durandetti; Perichon; Nedelec
Journal of Organic Chemistry, 2000 , vol. 65, # 15 p. 4575 - 4583
反应条件
tetra-n-butylammonium tetrafluoroborate; NiBr2bipy in N,N-dimethyl-formamide
T=60°C; electroreductive coupling; Electrochemical reaction;
参考文献
Cannes; Condon; Durandetti; Perichon; Nedelec
Journal of Organic Chemistry, 2000 , vol. 65, # 15 p. 4575 - 4583
反应条件
indium(III) chloride; indium; chloro-trimethyl-silane in tetrahydrofuran
T=25°C; 4 h;
参考文献
Ohe, Toshiyuki; Ohse, Takuya; Mori, Kenji; Ohtaka, Seiji; Uemura, Sakae
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 9 p. 1823 - 1827
反应条件
potassium tert-butylate in dimethyl sulfoxide
T=100°C; 0.5 h; stereoselective reaction;
参考文献
Trofimov, Boris A.; Schmidt, Elena Yu.; Zorina, Nadezhda V.; Ivanova, Elena V.; Ushakov, Igor A.
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 6880 - 6886
反应条件
water; toluene-4-sulfonic acid in acetone
T=50°C;
参考文献
Sutter
Tetrahedron Letters, 1989 , vol. 30, # 40 p. 5417 - 5420