反应条件
1: 59 percent / potassium dichromate, conc. sulphuric acid / H2O; diethyl ether / 0.5 h / -1 °C
2: 87 percent / ethanol / 40 - 50 °C
3: sodium cyanoborohydride / CH2Cl2; methanol / 2 h / 0 °C
4: 30percent aq. hydrogen peroxide, sodium peroxide / tetrahydrofuran / 24 h / Ambient temperature
View Scheme
参考文献
Bloodworth, A. J.; Courtneidge, J. L.; Curtis, Richard J.; Spencer, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 2951 - 2955