双[(三氟代甲基)磺酰基]甲烷合成路线 （共 20 条）
反应条件
bromine in dichloromethane; water Title compound not separated from byproducts.;
参考文献
Winter, Rolf W.; Gard
Journal of Fluorine Chemistry, 2006 , vol. 127, # 10 SPEC. ISS. p. 1324 - 1327
反应条件
dibenzoyl peroxide T=105 - 110°C; 72 h;
参考文献
Winter, Rolf W.; Gard
Journal of Fluorine Chemistry, 2006 , vol. 127, # 10 SPEC. ISS. p. 1324 - 1327
反应条件
in pentane
T=0°C; 1 h;
参考文献
Waller, Francis J.; Barrett, Anthony G. M.; Braddock, D. Christopher; Ramprasad, Dorai; McKinnell, R. Murray; White, Andrew J. P.; Williams, David J.; Ducray, Richard
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2910 - 2913
反应条件
in diethyl ether
1 h at 30-40°C, then 1.5 h at 35°C, 0.5 h at 50°C; acidification of the mixt. with 3 N HCl, distn. of the organic phase;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
dihydrogen peroxide; acetic acid
T=110°C; 10 h;
参考文献
Haas, Alois; Praas, Hans-Walter
Chemische Berichte, 1992 , vol. 125, # 3 p. 571 - 580
反应条件
dihydrogen peroxide; acetic acid
T=100°C; 12 h;
参考文献
Haas, Alois; Praas, Hans-Walter
Chemische Berichte, 1992 , vol. 125, # 3 p. 571 - 580
反应条件
1: bis(trifluoromethanesulfonyl)methane potassium salt With bromine in dichloromethane
2: vinylidene difluoride With dibenzoyl peroxide
T=75 - 85°C; 168 h; Further stages.;
参考文献
Winter, Rolf W.; Gard
Journal of Fluorine Chemistry, 2006 , vol. 127, # 10 SPEC. ISS. p. 1324 - 1327
参考文献
Koshar,R.J.; Mitsch,R.A.
Journal of Organic Chemistry, 1973 , vol. 38, p. 3358 - 3363
参考文献
Gramstad, T.; Haszeldine, R. N.
Journal of the Chemical Society, 1957 , p. 4069 - 4079
Full Text View citing articles Show Details
Minnesota Minning & Manufg. Co.
Patent: US2732398 , 1956 ;
C.A., 1956 , p. 13982
参考文献
Minnesota Mining and Mfg.Co.
Patent: US2732398 , 1954 ;
Full Text Show Details
Gramstad; Haszeldine
Journal of the Chemical Society, 1957 , p. 4069,4079
