双[(三氟代甲基)磺酰基]甲烷合成路线 （共 20 条）
反应条件
tri-n-butyl-antimony
参考文献
Pavlenko, N. V.; Yagupol'skii, Yu. L.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.1 p. 1148 - 1151
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1277 - 1280
参考文献
Koshar,R.J.; Mitsch,R.A.
Journal of Organic Chemistry, 1973 , vol. 38, p. 3358 - 3363
反应条件
ether, drying under Na2SO4 and isolation as (CF3SO2)2CHNa;
参考文献
Gramstad, T.; Haszeldine, R. N.
Journal of the Chemical Society, 1957 , p. 4069 - 4079
参考文献
Minnesota Mining and Manufacturing Company
Patent: US3932526 A1, 1976 ;
反应条件
in acetic anhydride
T=90°C; 12 h;
参考文献
Zhu
Synthesis, 1994 , # 3 p. 261 - 263
参考文献
Minnesota Mining and Manufacturing Company
Patent: US3932526 A1, 1976 ;
参考文献
Minnesota Mining and Manufacturing Company
Patent: US3932526 A1, 1976 ;
反应条件
in 1,2-dichloro-ethane
T=20°C; 5 h; Inert atmosphere;
参考文献
Yanai, Hikaru; Egawa, Saki; Taguchi, Takeo
Tetrahedron Letters, 2013 , vol. 54, # 17 p. 2160 - 2163
反应条件
in dichloromethane
T=40°C; 6 h; Inert atmosphere;
参考文献
Yanai, Hikaru; Ogura, Hiroshi; Fukaya, Haruhiko; Kotani, Akira; Kusu, Fumiyo; Taguchi, Takeo
Chemistry - A European Journal, 2011 , vol. 17, # 42 p. 11747 - 11751
反应条件
caesium chloride; tert.-butyl lithium
1) Et2O, -78 deg C, 1 h; 2) Et2O, -78 deg C --> rt, 2 h; 3) water; Yield givenMultistep reaction;
参考文献
Waller, Francis J.; Barrett, Anthony G. M.; Braddock, D. Christopher; Ramprasad, Dorai; McKinnell, R. Murray; White, Andrew J. P.; Williams, David J.; Ducray, Richard
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2910 - 2913
