1: 43 percent / PPA / 6 h / 110 °C
2: 80 percent / NaBH4 / methanol / 3 h / 20 °C
3: 71 percent / Et3SiH-BF3-OEt2 / CH2Cl2 / 15 h / 50 °C
View Scheme
参考文献
van Oeveren, Arjan; Pio, Barbara A.; Tegley, Christopher M.; Higuchi, Robert I.; Wu, Min; Jones, Todd K.; Marschke, Keith B.; Negro-Vilar, Andres; Zhi, Lin
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 6 p. 1523 - 1526
1: 72 percent / toluene / 20 h / Heating
2: 43 percent / PPA / 6 h / 110 °C
3: 80 percent / NaBH4 / methanol / 3 h / 20 °C
4: 71 percent / Et3SiH-BF3-OEt2 / CH2Cl2 / 15 h / 50 °C
View Scheme
参考文献
van Oeveren, Arjan; Pio, Barbara A.; Tegley, Christopher M.; Higuchi, Robert I.; Wu, Min; Jones, Todd K.; Marschke, Keith B.; Negro-Vilar, Andres; Zhi, Lin
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 6 p. 1523 - 1526
1: 72 percent / toluene / 20 h / Heating
2: 43 percent / PPA / 6 h / 110 °C
3: 80 percent / NaBH4 / methanol / 3 h / 20 °C
4: 71 percent / Et3SiH-BF3-OEt2 / CH2Cl2 / 15 h / 50 °C
View Scheme
参考文献
van Oeveren, Arjan; Pio, Barbara A.; Tegley, Christopher M.; Higuchi, Robert I.; Wu, Min; Jones, Todd K.; Marschke, Keith B.; Negro-Vilar, Andres; Zhi, Lin
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 6 p. 1523 - 1526
