N-甲基-N-苯基氨基甲酰氯合成路线 （共 46 条）
反应条件
in toluene 1.) room temperature, 1 h, 2.) reflux, 1.5 h;
参考文献
Freer, Richard; McKillop, Alexander
Synthetic Communications, 1996 , vol. 26, # 2 p. 331 - 349
反应条件
sodium hydroxide 0.0833333 h; Neat (no solvent);
参考文献
Zare, Hassan; Ghanbari, Mohammad Mehdi; Jamali, Marzieh; Aboodi, Abdollah
Chinese Chemical Letters, 2012 , vol. 23, # 8 p. 883 - 886
反应条件
sulfuryl dichloride in chloroform-d1 T=25°C; 72 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
1: 25 percent / Na2CO3 / CH2Cl2; H2O / 72 h / 20 °C 2: 44 percent / 0.5 h View Scheme
参考文献
Lemoucheux, Laurent; Rouden, Jacques; Ibazizene, Meziane; Sobrio, Franck; Lasne, Marie-Claire
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7289 - 7297
反应条件
sulfuryl dichloride in chloroform-d1 T=25°C; 72 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
sulfuryl dichloride in chloroform-d1 T=25°C; 72 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
sulfuryl dichloride in chloroform-d1 T=25°C;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
1: With sulfuryl dichloride in chloroform-d1 T=25°C; 2: in chloroform-d1; methanol-d4 2 h;
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
1: acetonitrile / 24 h / 105 °C 2: chloroform-d1 / 24 h / 4 - 25 °C 3: sulfuryl dichloride / chloroform-d1 / 25 °C View Scheme
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
反应条件
1: O-isopropyl N-methyl-N-phenylthiocarbamate With sulfuryl dichloride in chloroform-d1 T=25°C; 2: in chloroform-d1; methanol-d4 2 h; 3: N-methylaniline in chloroform-d1; methanol-d4
参考文献
Schrader, Alex M.; Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7882 - 7892
