2-甲基-1,5-戊烷二醇合成路线 （共 14 条）
反应条件
Amberlyst 15 T=140 - 160°C;
参考文献
Eliel,E.L.; Hargrave,K.; Pietrusiewisz,K.
Journal of the American Chemical Society, 1982 , vol. 104, p. 3635
反应条件
Amberlyst 15 T=140 - 160°C;
参考文献
Eliel,E.L.; Hargrave,K.; Pietrusiewisz,K.
Journal of the American Chemical Society, 1982 , vol. 104, p. 3635
反应条件
triethylamine; 4-phenylbut-3-en-2-one; Ru2Cl4(1,4-bis(diphenylphosphino)butane)3 in toluene T=140°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Ishii, Youichi; Osakada, Kohtaro; Ikariya, Takao; Saburi, Masahiko; Yoshikawa, Sadao
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2034 - 2039
反应条件
C13H31BS in tetrahydrofuran
T=20°C; 18 h;
参考文献
Patra, Pranab K.; Nishide, Kiyoharu; Fuji, Kaoru; Node, Manabu
Synthesis, 2004 , # 7 p. 1003 - 1006
反应条件
copper oxide-chromium oxide
Hydrogenation;
参考文献
Whitehead et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3632
反应条件
hydrogen; nickel; acetic acid
T=105°C; P=62518.2 Torr;
参考文献
N.V.de Bataafsche Petr.Mij.
Patent: DE1003704 , 1950 ;
Full Text Show Details
Shell Devel.Co.
Patent: US2546019 , 1947 ;
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Julia,M.; Maumy,M.
Bulletin de la Societe Chimique de France, 1969 , p. 2415 - 2427
反应条件
1: 79 percent / Et3N / diethyl ether / a) O dge C, 30 min, b) RT, 12 h
2: 1.) H2, tetrakis(acetato)dirhodium(II) (<Rh(OAc)2>2), 2.) LAH / 1.) benzene, 500 psi, 2.) ether, water
View Scheme
参考文献
Jackson, W. Roy; Moffat, Mark R.; Perlmutter, Patrick; Tasdelen, E. Elizabeth
Australian Journal of Chemistry, 1992 , vol. 45, # 5 p. 823 - 834
反应条件
1: aq. HCl
2: LiAlH4 / diethyl ether
View Scheme
参考文献
Julia,M.; Maumy,M.
Bulletin de la Societe Chimique de France, 1969 , p. 2415 - 2427
参考文献
Hanschke
Chemische Berichte, 1955 , vol. 88, p. 1053,1059
