3,5-二氧代环己烷羧酸合成路线 (共 11 条)
反应条件
hydrogen; sodium hydroxide T=70°C; P=38787.1 Torr;
参考文献
Seo, Young Ho; Carroll, Kate S.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 2 p. 356 - 359
参考文献
Birch et al.
Australian Journal of Chemistry, 1954 , vol. 7, p. 256,259
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Kuehne; Lambert
Journal of the American Chemical Society, 1959 , vol. 81, p. 4278,4283
Organic Syntheses, 1973 , vol. Coll. Vol. V, p. 400
反应条件
1: toluene-4-sulfonic acid; benzene 2: LiAlH4 View Scheme
参考文献
van Tamelen; Hildahl
Journal of the American Chemical Society, 1956 , vol. 78, p. 4405,4410
反应条件
1: aqueous KOH 2: diethylene glycol; hydrazine hydrate; methanol / 195 °C / Reagens 4: Natriumhydroxid View Scheme
参考文献
Stetter; Meisel
Chemische Berichte, 1957 , vol. 90, p. 2928,2930
反应条件
1: toluene-4-sulfonic acid; benzene 2: LiAlH4 4: diethyl ether; NaOH; water 5: air; aq. NaOH solution View Scheme
参考文献
Journal of the American Chemical Society, , vol. 78, p. 4405,4410
反应条件
hydrogenchloride in tetrahydrofuran; ethyl acetate
参考文献
Ciba-Geigy Corporation
Patent: US4618360 A1, 1986 ;
反应条件
potassium hydroxide; copper
参考文献
Stetter; Meisel
Chemische Berichte, 1957 , vol. 90, p. 2928,2930
反应条件
sulfuric acid
Ambient temperature;
参考文献
Mokbel, Luci; Savage, G. Paul; Simpson, Gregory W.
Australian Journal of Chemistry, 1994 , vol. 47, # 9 p. 1727 - 1734
参考文献
Stetter; Meisel
Chemische Berichte, 1957 , vol. 90, p. 2928,2930
反应条件
sodium hydroxide; hydrazine hydrate
T=195°C;
参考文献
Stetter; Meisel
Chemische Berichte, 1957 , vol. 90, p. 2928,2930