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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-萘乙胺
合成路线
（共 56 条）
344248-49-3
→
反应条件
42882-31-5
1-萘乙胺
反应条件
hydrogenchloride in ethanol T=20°C; 2 h;
参考文献
Avecia Limited
Patent: US6696608 B1, 2004 ;
Location in patent: Page column 28 ;
941-98-0
1-乙酰基萘
→
反应条件
42882-31-5
1-萘乙胺
反应条件
hydroxylamine hydrochloride; ammonium formate; zinc in methanol 5 h; Reflux;
参考文献
Falus, Peter; Boros, Zoltan; Hornyanszky, Gabor; Nagy, Jozsef; Darvas, Ferenc; Uerge, Laszlo; Poppe, Laszlo
Tetrahedron Letters, 2011 , vol. 52, # 12 p. 1310 - 1312
1956-40-7
1-(1-萘)-乙酮肟
→
反应条件
42882-31-5
1-萘乙胺
反应条件
ammonia; hydrogen in methanol; water T=58 - 62°C; P=2574.5 - 2942.29 Torr;
参考文献
Mathad, Vijayavitthal T.; Shinde, Gorakshanath B.; Ippar, Sharad S.; Niphade, Navnath C.; Panchangam, Raghavendra K.; Vankawala, Pravinchandra J.
Synthetic Communications, 2011 , vol. 41, # 3 p. 341 - 346
10420-89-0
(S)-(-)-1-(1-萘基)乙胺
→
反应条件
946113-79-7
+
42882-31-5
1-萘乙胺
反应条件
Raney Co; hydrogen in toluene T=70°C; P=150.015 Torr; 72 h; Autoclave;
参考文献
Parvulescu, Andrei N.; Jacobs, Pierre A.; De Vos, Dirk E.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 1 p. 113 - 121
3886-70-2
(R)-1-(1-萘基)乙胺
→
反应条件
42882-31-5
1-萘乙胺
反应条件
ammonia; hydrogen T=175°C; P=46504.7 - 50255 Torr; 12 h; Autoclave; Catalytic behavior; ConcentrationPressure;
参考文献
SCHREMS, Marcus Georg
Patent: US2013/345475 A1, 2013 ;
Location in patent: Paragraph 0117 ;
3886-70-2
(R)-1-(1-萘基)乙胺
→
反应条件
1127-76-0
1-乙基萘
+
42882-31-5
1-萘乙胺
反应条件
ammonia; hydrogen T=200°C; P=46504.7 - 50255 Torr; 12 h; Autoclave; Catalytic behavior;
参考文献
SCHREMS, Marcus Georg
Patent: US2013/345475 A1, 2013 ;
Location in patent: Paragraph 0116 ;
42882-31-5
1-萘乙胺
→
反应条件
941-98-0
1-乙酰基萘
反应条件
oxalic acid; dimethyl sulfoxide; phenylphosphoric acid dichloride; triethylamine 1.) -10 deg C, 15 min, CH2Cl2, 2.) -10 deg C to 20 deg C, 45 min, 3.) 20 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Leisch, Hannes; Grosse, Stephan; Iwaki, Hiroaki; Hasegawa, Yoshie; Lau, Peter C.K.
Canadian Journal of Chemistry, 2012 , vol. 90, # 1 p. 39 - 45
42882-31-5
1-萘乙胺
→
反应条件
941-98-0
1-乙酰基萘
+
3886-70-2
(R)-1-(1-萘基)乙胺
反应条件
2,6-dimethylpyridine; chiral 1-azaspiro[5.5]undecane N-oxyl radical; sodium perchlorate in water; acetonitrile Oxidation; 5 h; Electrolysis;
参考文献
Truppo, Matthew D.; Turner, Nicholas J.; Rozzell, J. David
Chemical Communications, 2009 , # 16 p. 2127 - 2129
42882-31-5
1-萘乙胺
→
反应条件
941-98-0
1-乙酰基萘
+
10420-89-0
(S)-(-)-1-(1-萘基)乙胺
反应条件
D-amino acid oxidase; ATA-117; pyridoxal 5'-phosphate; 2-oxo-propionic acid T=30°C; pH=8; 3 h; Resolution of racemateaq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Truppo, Matthew D.; Turner, Nicholas J.; Rozzell, J. David
Chemical Communications, 2009 , # 16 p. 2127 - 2129
42882-31-5
1-萘乙胺
→
反应条件
10420-89-0
(S)-(-)-1-(1-萘基)乙胺
+
3886-70-2
(R)-1-(1-萘基)乙胺
反应条件
1: With (S)-isopropylidene glycerol 3-carboxy-2-naphthoate in methanol T=20°C; 2: With sulfuric acid in ethyl acetate
参考文献
Pallavicini, Marco; Bolchi, Cristiano; Fumagalli, Laura; Valoti, Ermanno; Villa, Luigi
Tetrahedron Asymmetry, 2002 , vol. 13, # 20 p. 2277 - 2282
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