N-苄基-2-甲基-1-丙胺合成路线 (共 18 条)
反应条件
sodium amalgam; ethanol
参考文献
Zaunschirm
Justus Liebigs Annalen der Chemie, 1888 , vol. 245, p. 285
反应条件
3 platinum on carbon; hydrogen in toluene
T=105°C; P=4500.45 Torr; Flow reactor;
参考文献
Sharma, Sumeet K.; Lynch, James; Sobolewska, Anna M.; Plucinski, Pawel; Watson, Robert J.; Williams, Jonathan M. J.
Catalysis Science and Technology, 2013 , vol. 3, # 1 p. 85 - 88
反应条件
3 platinum on carbon; hydrogen in toluene
T=105°C; P=4500.45 Torr; Flow reactor;
参考文献
Sharma, Sumeet K.; Lynch, James; Sobolewska, Anna M.; Plucinski, Pawel; Watson, Robert J.; Williams, Jonathan M. J.
Catalysis Science and Technology, 2013 , vol. 3, # 1 p. 85 - 88
反应条件
titanocene dichloride; n-butyl-magnesium chloride in diethyl ether
T=25°C; 15 h;
参考文献
Amin, Sk. Rasidul; Crowe, William E.
Tetrahedron Letters, 1997 , vol. 38, # 43 p. 7487 - 7490
反应条件
1: With manganese(IV) oxide; sodium tetrahydroborate in dichloromethane
18 h; Heating;
2: With methanol
T=0 - 20°C; 0.666667 h;
参考文献
Kanno, Hisashi; Taylor, Richard J.K.
Tetrahedron Letters, 2002 , vol. 43, # 41 p. 7337 - 7340
反应条件
4 A molecular sieve; borane-pyridine complex in methanol
16 h;
参考文献
Bomann, Mark D.; Guch, Ian C.; DiMare, Marcello
Journal of Organic Chemistry, 1995 , vol. 60, # 18 p. 5995 - 5996
反应条件
1: With manganese(IV) oxide; polymer-bound trimethyl ammonium cyanoborohydride in dichloromethane
Heating;
2: With acetic acid
Heating; Further stages.;
参考文献
Blackburn, Leonie; Taylor, Richard J. K.
Organic Letters, 2001 , vol. 3, # 11 p. 1637 - 1639
反应条件
1: With samarium diiodide in tetrahydrofuran
T=20°C; P=37503.8 Torr; 16 h; Autoclave;
2: With trifluoroacetic acid in tetrahydrofuran; water
参考文献
Prikhod'Ko, Alexander; Walter, Olaf; Zevaco, Thomas A.; Garcia-Rodriguez, Jaime; Mouhtady, Omar; Py, Sandrine
European Journal of Organic Chemistry, 2012 , # 20 p. 3742 - 3746
反应条件
hydrogen; magnesium oxide; copper
T=210°C; P=7500.6 Torr;
参考文献
Tarasevich; Kozlov
Russian Journal of General Chemistry, 2004 , vol. 74, # 3 p. 379 - 383
反应条件
1: With samarium diiodide in tetrahydrofuran
T=20°C; P=37503.8 Torr; 16 h; Autoclave;
2: With trifluoroacetic acid in tetrahydrofuran; water
参考文献
Prikhod'Ko, Alexander; Walter, Olaf; Zevaco, Thomas A.; Garcia-Rodriguez, Jaime; Mouhtady, Omar; Py, Sandrine
European Journal of Organic Chemistry, 2012 , # 20 p. 3742 - 3746