N-苄基-2-甲基-1-丙胺合成路线 (共 18 条)
参考文献
Petrolite Corporation
Patent: US4235809 A1, 1980 ;
反应条件
1: manganese dioxide / CH2Cl2 / Heating
2: sodium borohydride / methanol / 0.33 h / 0 °C
View Scheme
参考文献
Blackburn, Leonie; Taylor, Richard J. K.
Organic Letters, 2001 , vol. 3, # 11 p. 1637 - 1639
反应条件
1: With samarium diiodide in tetrahydrofuran
T=-78 - 20°C;
2: With trifluoroacetic acid in tetrahydrofuran; water
参考文献
Prikhod'Ko, Alexander; Walter, Olaf; Zevaco, Thomas A.; Garcia-Rodriguez, Jaime; Mouhtady, Omar; Py, Sandrine
European Journal of Organic Chemistry, 2012 , # 20 p. 3742 - 3746
参考文献
Petrolite Corporation
Patent: US4442286 A1, 1984 ;
反应条件
1: 78 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 24 h / Ambient temperature
2: lithium aluminum hydride / diethyl ether / Heating
View Scheme
参考文献
Kathryn, E. Bell; Knight, David W.; Gravestock, Michael B.
Tetrahedron Letters, 1995 , vol. 36, # 47 p. 8681 - 8684
反应条件
1: benzene
2: LiAlH4 / diethyl ether / Heating
View Scheme
参考文献
Vejdelek,Z.J. et al.
Collection of Czechoslovak Chemical Communications, 1972 , vol. 37, p. 3501 - 3511
反应条件
1: 52 percent / toluene / 24 h / Heating
2: 75 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Heating
View Scheme
参考文献
Katritzky, Alan R.; Drewniak, Malgorzata
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2339 - 2344
参考文献
Redmore,D.
Journal of Organic Chemistry, 1978 , vol. 43, p. 992 - 996